C₂₃H₂₂ClNO₅S

Base Information

Chemical Name:C₂₃H₂₂ClNO₅S
CAS No.:1374779-33-5
Molecular Formula:C₂₃H₂₂ClNO₅S
Molecular Weight:459.95
Hs Code.:

C<sub>23</sub>H<sub>22</sub>ClNO<sub>5</sub>S

Synonyms:C₂₃H₂₂ClNO₅S

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Chemical Property of C₂₃H₂₂ClNO₅S

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Technology Process of C₂₃H₂₂ClNO₅S

There total 4 articles about C₂₃H₂₂ClNO₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374779-32-4
C₂₂H₂₀ClNO₅S

: 74-88-4
methyl iodide

: 1374779-33-5
C₂₃H₂₂ClNO₅S

Guidance literature:: C₂₂H₂₀ClNO₅S; With sodium hydride; In tetrahydrofuran; at 0 - 5 ℃; for 1h;

methyl iodide; In tetrahydrofuran; at 20 ℃; for 12h;

Reference yield:

: 35092-89-8
4-(methoxycarbonyl)-3-nitrobenzoic acid

: 1374779-33-5
C₂₃H₂₂ClNO₅S

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / 1,4-dioxane / 48 h / -15 °C

2.1: hydrogen / palladium 10% on activated carbon / methanol / 20 h / -15 °C

3.1: hydrogen / tetrahydrofuran / 14 h / Reflux

4.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 5 °C

4.2: 12 h / 20 °C

With sulfuric acid; hydrogen; sodium hydride; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol;

Reference yield:

: 147291-52-9
tert-butyl 4-(methoxycarbonyl)-3-nitrobenzoate

: 1374779-33-5
C₂₃H₂₂ClNO₅S

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen / palladium 10% on activated carbon / methanol / 20 h / -15 °C

2.1: hydrogen / tetrahydrofuran / 14 h / Reflux

3.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 5 °C

3.2: 12 h / 20 °C

With hydrogen; sodium hydride; palladium 10% on activated carbon; In tetrahydrofuran; methanol;