(2E)-3-{4-[(6-{3-[(1E)-2-cyano-2-(5-formylthiophen-2-yl)eth-1-en-1-yl]-10H-phenothiazin-10-yl}hexyl)(phenyl)amino]phenyl}-2-(5-formylthiophen-2-yl)prop-2-enenitrile

Base Information

Chemical Name:(2E)-3-{4-[(6-{3-[(1E)-2-cyano-2-(5-formylthiophen-2-yl)eth-1-en-1-yl]-10H-phenothiazin-10-yl}hexyl)(phenyl)amino]phenyl}-2-(5-formylthiophen-2-yl)prop-2-enenitrile
CAS No.:1376330-06-1
Molecular Formula:C₄₆H₃₆N₄O₂S₃
Molecular Weight:773.015
Hs Code.:

(2E)-3-{4-[(6-{3-[(1E)-2-cyano-2-(5-formylthiophen-2-yl)eth-1-en-1-yl]-10H-phenothiazin-10-yl}hexyl)(phenyl)amino]phenyl}-2-(5-formylthiophen-2-yl)prop-2-enenitrile

Synonyms:(2E)-3-{4-[(6-{3-[(1E)-2-cyano-2-(5-formylthiophen-2-yl)eth-1-en-1-yl]-10H-phenothiazin-10-yl}hexyl)(phenyl)amino]phenyl}-2-(5-formylthiophen-2-yl)prop-2-enenitrile

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Chemical Property of (2E)-3-{4-[(6-{3-[(1E)-2-cyano-2-(5-formylthiophen-2-yl)eth-1-en-1-yl]-10H-phenothiazin-10-yl}hexyl)(phenyl)amino]phenyl}-2-(5-formylthiophen-2-yl)prop-2-enenitrile

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Technology Process of (2E)-3-{4-[(6-{3-[(1E)-2-cyano-2-(5-formylthiophen-2-yl)eth-1-en-1-yl]-10H-phenothiazin-10-yl}hexyl)(phenyl)amino]phenyl}-2-(5-formylthiophen-2-yl)prop-2-enenitrile

There total 6 articles about (2E)-3-{4-[(6-{3-[(1E)-2-cyano-2-(5-formylthiophen-2-yl)eth-1-en-1-yl]-10H-phenothiazin-10-yl}hexyl)(phenyl)amino]phenyl}-2-(5-formylthiophen-2-yl)prop-2-enenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.7%

: 1376330-04-9
(2E)-3-{4-[(6-{3-[(1E)-2-cyano-2-(thiophen-2-yl)eth-1-en-1-yl]-10H-phenothiazin-10-yl}hexyl)(phenyl)amino]phenyl}-2-(thiophen-2-yl)prop-2-enenitrile

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1376330-06-1
(2E)-3-{4-[(6-{3-[(1E)-2-cyano-2-(5-formylthiophen-2-yl)eth-1-en-1-yl]-10H-phenothiazin-10-yl}hexyl)(phenyl)amino]phenyl}-2-(5-formylthiophen-2-yl)prop-2-enenitrile

Guidance literature:: With trichlorophosphate; In 1,2-dichloro-ethane; at 0 - 90 ℃; for 4h; Inert atmosphere; Reflux;
DOI:10.1016/j.dyepig.2012.02.011

Reference yield:

: 1376329-98-4
(6-phenothiazin-10-yl-hexyl)diphenylamine

: 1376330-06-1
(2E)-3-{4-[(6-{3-[(1E)-2-cyano-2-(5-formylthiophen-2-yl)eth-1-en-1-yl]-10H-phenothiazin-10-yl}hexyl)(phenyl)amino]phenyl}-2-(5-formylthiophen-2-yl)prop-2-enenitrile

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / 1,2-dichloro-ethane / 4 h / 0 - 90 °C

2: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere; Reflux

3: trichlorophosphate / 1,2-dichloro-ethane / 4 h / 0 - 90 °C / Inert atmosphere; Reflux

With potassium tert-butylate; trichlorophosphate; In tetrahydrofuran; 1,2-dichloro-ethane; 1: Vilsmeier-Haack reaction / 2: Knoevenagel condensation / 3: Vilsmeier-Haack reaction;
DOI:10.1016/j.dyepig.2012.02.011

Reference yield:

: 629-03-8
1 ,6-dibromohexane

: 1376330-06-1
(2E)-3-{4-[(6-{3-[(1E)-2-cyano-2-(5-formylthiophen-2-yl)eth-1-en-1-yl]-10H-phenothiazin-10-yl}hexyl)(phenyl)amino]phenyl}-2-(5-formylthiophen-2-yl)prop-2-enenitrile

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / 1,2-dimethoxyethane / 0.5 h / 20 °C / Inert atmosphere

1.2: 2 h / 85 °C / Inert atmosphere

2.1: potassium hydroxide / dimethyl sulfoxide / 0.17 h / Inert atmosphere

2.2: 4 h / 20 °C / Inert atmosphere

3.1: trichlorophosphate / 1,2-dichloro-ethane / 4 h / 0 - 90 °C

4.1: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere; Reflux

5.1: trichlorophosphate / 1,2-dichloro-ethane / 4 h / 0 - 90 °C / Inert atmosphere; Reflux

With potassium tert-butylate; sodium hydride; potassium hydroxide; trichlorophosphate; In tetrahydrofuran; 1,2-dimethoxyethane; dimethyl sulfoxide; 1,2-dichloro-ethane; 3.1: Vilsmeier-Haack reaction / 4.1: Knoevenagel condensation / 5.1: Vilsmeier-Haack reaction;
DOI:10.1016/j.dyepig.2012.02.011