(2,3,4,5,6-pentafluorophenyl)methyl 10-(2-aza-2-methoxy-1-methylvinyl)-11-(2-aza-2-methoxyvinyl)-14-hydroxynonadeca-4(Z),7(Z),12(E),16(Z)-tetraenoate

Base Information

Chemical Name:(2,3,4,5,6-pentafluorophenyl)methyl 10-(2-aza-2-methoxy-1-methylvinyl)-11-(2-aza-2-methoxyvinyl)-14-hydroxynonadeca-4(Z),7(Z),12(E),16(Z)-tetraenoate
CAS No.:291545-31-8
Molecular Formula:C₃₁H₃₉F₅N₂O₅
Molecular Weight:614.653
Hs Code.:

Synonyms:(2,3,4,5,6-pentafluorophenyl)methyl 10-(2-aza-2-methoxy-1-methylvinyl)-11-(2-aza-2-methoxyvinyl)-14-hydroxynonadeca-4(Z),7(Z),12(E),16(Z)-tetraenoate

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Chemical Property of (2,3,4,5,6-pentafluorophenyl)methyl 10-(2-aza-2-methoxy-1-methylvinyl)-11-(2-aza-2-methoxyvinyl)-14-hydroxynonadeca-4(Z),7(Z),12(E),16(Z)-tetraenoate

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Technology Process of (2,3,4,5,6-pentafluorophenyl)methyl 10-(2-aza-2-methoxy-1-methylvinyl)-11-(2-aza-2-methoxyvinyl)-14-hydroxynonadeca-4(Z),7(Z),12(E),16(Z)-tetraenoate

There total 3 articles about (2,3,4,5,6-pentafluorophenyl)methyl 10-(2-aza-2-methoxy-1-methylvinyl)-11-(2-aza-2-methoxyvinyl)-14-hydroxynonadeca-4(Z),7(Z),12(E),16(Z)-tetraenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1765-40-8
(bromomethyl)pentafluorobenzene

: 291545-30-7
10-(2-aza-2-methoxy-1-methylvinyl)-11-(2-aza-2-methoxyvinyl)-14-hydroxynonadeca-4(Z),7(Z),12(E),16(Z)-tetraenoic acid

: 291545-31-8
(2,3,4,5,6-pentafluorophenyl)methyl 10-(2-aza-2-methoxy-1-methylvinyl)-11-(2-aza-2-methoxyvinyl)-14-hydroxynonadeca-4(Z),7(Z),12(E),16(Z)-tetraenoate

Guidance literature:: With diisopropylamine; In acetonitrile; at 20 ℃; for 8h;
DOI:10.1021/jo000537v

Reference yield:

: 291545-26-1
10-acetyl-11-formyl-14-hydroxynonadeca-4(Z),7(Z),12(E),16(Z)-tetraenoic acid

: 291545-31-8
(2,3,4,5,6-pentafluorophenyl)methyl 10-(2-aza-2-methoxy-1-methylvinyl)-11-(2-aza-2-methoxyvinyl)-14-hydroxynonadeca-4(Z),7(Z),12(E),16(Z)-tetraenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / pyridine / 15 h / 20 °C

2: 85 percent / diisopropylamine / acetonitrile / 8 h / 20 °C

With diisopropylamine; In pyridine; acetonitrile; 1: Condensation / 2: Alkylation;
DOI:10.1021/jo000537v

Reference yield:

: (4Z,7Z,12E,16Z)-(S)-10-Acetyl-14-(tert-butyl-dimethyl-silanyloxy)-11-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-nonadeca-4,7,12,16-tetraenoic acid

: 291545-31-8
(2,3,4,5,6-pentafluorophenyl)methyl 10-(2-aza-2-methoxy-1-methylvinyl)-11-(2-aza-2-methoxyvinyl)-14-hydroxynonadeca-4(Z),7(Z),12(E),16(Z)-tetraenoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: aq. AcOH; butylated hydroxytoluene / 4 h / 40 °C

1.2: 3.8 mg / sodium metaperiodate / acetone; H₂O; acetic acid / 1.8 h / 20 °C

2.1: 81 percent / pyridine / 15 h / 20 °C

3.1: 85 percent / diisopropylamine / acetonitrile / 8 h / 20 °C

With 2,6-di-tert-butyl-4-methyl-phenol; acetic acid; diisopropylamine; In pyridine; acetonitrile; 1.1: desilylation; deketalization / 1.2: Oxidation / 2.1: Condensation / 3.1: Alkylation;
DOI:10.1021/jo000537v