C₂₈H₃₅N₅O₅

Base Information

Chemical Name:C₂₈H₃₅N₅O₅
CAS No.:1298101-49-1
Molecular Formula:C₂₈H₃₅N₅O₅
Molecular Weight:521.616
Hs Code.:

C<sub>28</sub>H<sub>35</sub>N<sub>5</sub>O<sub>5</sub>

Synonyms:C₂₈H₃₅N₅O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₃₅N₅O₅

Chemical Property:

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Technology Process of C₂₈H₃₅N₅O₅

There total 4 articles about C₂₈H₃₅N₅O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1259278-17-5,1788036-28-1,609788-04-7,849616-22-4
tert-butyl N-[(1R,3S)-3-aminocyclohexyl]carbamate

: 1298101-48-0
5-chloro-4-(4-methoxy-phenoxy)-2-(5-methoxy-pyridin-3-yl)-pyrimidine

: 1298101-49-1
C₂₈H₃₅N₅O₅

Guidance literature:: With caesium carbonate; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In 1,4-dioxane; at 95 ℃; for 3h; tube sealed with a teflon-lined septum; Inert atmosphere;

Reference yield:

: 347186-01-0,1788036-28-1,609788-04-7,849616-22-4
N-(3-aminocyclohexyl)(t-butoxy)carboxamide

: 1298101-49-1
C₂₈H₃₅N₅O₅

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / -20 - 20 °C / Inert atmosphere

2: CHIRALPAK_.(R). AD_.(TM). column / isopropyl alcohol; hexane / Resolution of racemate

3: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 2068.65 Torr

4: caesium carbonate / 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 3 h / 95 °C / tube sealed with a teflon-lined septum; Inert atmosphere

With hydrogen; caesium carbonate; N-ethyl-N,N-diisopropylamine; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium 10% on activated carbon; In 1,4-dioxane; methanol; hexane; dichloromethane; isopropyl alcohol;

Reference yield:

: (±)-cis-3-((tert-butoxycarbonyl)amino)-1-benzoxyformamidocyclohexane

: 1298101-49-1
C₂₈H₃₅N₅O₅

Guidance literature:: Multi-step reaction with 3 steps

1: CHIRALPAK_.(R). AD_.(TM). column / isopropyl alcohol; hexane / Resolution of racemate

2: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 2068.65 Torr

3: caesium carbonate / 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 3 h / 95 °C / tube sealed with a teflon-lined septum; Inert atmosphere

With hydrogen; caesium carbonate; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium 10% on activated carbon; In 1,4-dioxane; methanol; hexane; isopropyl alcohol;