Technology Process of C8H11N*C12H14O3
There total 4 articles about C8H11N*C12H14O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
acetone;
at 20 ℃;
boiling;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: zinc; iodine / copper(l) chloride / tetrahydrofuran / 1.25 h / 20 °C / Inert atmosphere; Reflux
2.1: hydrogen / palladium 10% on activated carbon / ethanol / 20 °C
3.1: water; lithium hydroxide monohydrate / 1,4-dioxane / 20 °C
3.2: pH 1
4.1: acetone / 20 °C / boiling
With
lithium hydroxide monohydrate; water; hydrogen; iodine; zinc;
palladium 10% on activated carbon; copper(l) chloride;
In
tetrahydrofuran; 1,4-dioxane; ethanol; acetone;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogen / palladium 10% on activated carbon / ethanol / 20 °C
2.1: water; lithium hydroxide monohydrate / 1,4-dioxane / 20 °C
2.2: pH 1
3.1: acetone / 20 °C / boiling
With
lithium hydroxide monohydrate; water; hydrogen;
palladium 10% on activated carbon;
In
1,4-dioxane; ethanol; acetone;