[nickel(II) (N-methyl-1,4-diazacycloheptane) (benzoylacetonate)2]

Base Information

Chemical Name:[nickel(II) (N-methyl-1,4-diazacycloheptane) (benzoylacetonate)2]
CAS No.:942411-91-8
Molecular Formula:C₂₆H₃₂N₂NiO₄
Molecular Weight:495.241
Hs Code.:

Synonyms:[nickel(II) (N-methyl-1,4-diazacycloheptane) (benzoylacetonate)2]

Suppliers and Price of [nickel(II) (N-methyl-1,4-diazacycloheptane) (benzoylacetonate)2]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [nickel(II) (N-methyl-1,4-diazacycloheptane) (benzoylacetonate)2]

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Technology Process of [nickel(II) (N-methyl-1,4-diazacycloheptane) (benzoylacetonate)2]

There total 1 articles about [nickel(II) (N-methyl-1,4-diazacycloheptane) (benzoylacetonate)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4318-37-0
1-Methylhomopiperazine

: nickel(II) sulfate hexahydrate

: 93-91-4
1-phenylbutan-1,3-dione

: 942411-91-8
[nickel(II) (N-methyl-1,4-diazacycloheptane) (benzoylacetonate)2]

Guidance literature:: With Na₂CO₃; In chloroform; water; NiSO4*6H2O dissolved in water; chloroform soln. of equimolar amount of cyclic ligand and 2 molar amount of diketone added to it in a separatory funnel; Na2CO3 added to the mixture with shaking; after standing a minute, chloroform layer separated and evaporated; crude crystals recrystallized from DCE; elem. anal.;
DOI:10.1016/j.poly.2006.11.003