C₂₅H₁₅I₂NO₅

Base Information

Chemical Name:C₂₅H₁₅I₂NO₅
CAS No.:1426329-99-8
Molecular Formula:C₂₅H₁₅I₂NO₅
Molecular Weight:663.207
Hs Code.:

C<sub>25</sub>H<sub>15</sub>I<sub>2</sub>NO<sub>5</sub>

Synonyms:C₂₅H₁₅I₂NO₅

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Chemical Property of C₂₅H₁₅I₂NO₅

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Technology Process of C₂₅H₁₅I₂NO₅

There total 8 articles about C₂₅H₁₅I₂NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1426329-98-7
7-(4-hydroxy-3,5-diiodophenyl)-3,8-bis(4-methoxyphenyl)-1H-pyrrolo[2,1-c][1,4]oxazin-1-one

: 1426329-99-8
C₂₅H₁₅I₂NO₅

Guidance literature:: With boron tribromide; In dichloromethane; at -78 ℃; for 12.5h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2013.01.077

Reference yield:

: 1426329-89-6
benzyl N-benzenesulfonyl-3-bromo-4-(4-isopropoxyphenyl)pyrrole-2-carboxylate

: 1426329-99-8
C₂₅H₁₅I₂NO₅

Guidance literature:: Multi-step reaction with 8 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; 1,2-dimethoxyethane / 15 h / 85 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Reflux

3: potassium carbonate / N,N-dimethyl-formamide / 3 h / 70 °C

4: palladium on carbon; hydrogen / ethyl acetate / 7 h / 20 °C

5: sodium acetate / acetic anhydride / 1.5 h / 100 °C

6: boron trichloride / dichloromethane; n-heptane / 2 h / -78 - 0 °C

7: N-iodosaccharine; ammonia / N,N-dimethyl-formamide; ethanol / 2 h / 0 °C

8: boron tribromide / dichloromethane / 12.5 h / -78 °C / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-iodosaccharine; palladium on carbon; tetrabutyl ammonium fluoride; ammonia; hydrogen; sodium acetate; boron trichloride; boron tribromide; sodium carbonate; potassium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; n-heptane; dichloromethane; water; acetic anhydride; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2013.01.077

Reference yield:

: 5720-07-0
4-methoxyphenylboronic acid

: 1426329-99-8
C₂₅H₁₅I₂NO₅

Guidance literature:: Multi-step reaction with 8 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; 1,2-dimethoxyethane / 15 h / 85 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Reflux

3: potassium carbonate / N,N-dimethyl-formamide / 3 h / 70 °C

4: palladium on carbon; hydrogen / ethyl acetate / 7 h / 20 °C

5: sodium acetate / acetic anhydride / 1.5 h / 100 °C

6: boron trichloride / dichloromethane; n-heptane / 2 h / -78 - 0 °C

7: N-iodosaccharine; ammonia / N,N-dimethyl-formamide; ethanol / 2 h / 0 °C

8: boron tribromide / dichloromethane / 12.5 h / -78 °C / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-iodosaccharine; palladium on carbon; tetrabutyl ammonium fluoride; ammonia; hydrogen; sodium acetate; boron trichloride; boron tribromide; sodium carbonate; potassium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; n-heptane; dichloromethane; water; acetic anhydride; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2013.01.077