C₄₀H₄₅N₃O₈SSi

Base Information

Chemical Name:C₄₀H₄₅N₃O₈SSi
CAS No.:1314716-27-2
Molecular Formula:C₄₀H₄₅N₃O₈SSi
Molecular Weight:755.964
Hs Code.:

C<sub>40</sub>H<sub>45</sub>N<sub>3</sub>O<sub>8</sub>SSi

Synonyms:C₄₀H₄₅N₃O₈SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₀H₄₅N₃O₈SSi

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Technology Process of C₄₀H₄₅N₃O₈SSi

There total 16 articles about C₄₀H₄₅N₃O₈SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.2%

: 1314716-25-0
C₃₄H₃₁N₃O₈S

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1314716-27-2
C₄₀H₄₅N₃O₈SSi

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 20h;

Reference yield:

: 1314716-21-6
C₃₈H₄₄O₁₀SSi

: 1314716-27-2
C₄₀H₄₅N₃O₈SSi

Guidance literature:: Multi-step reaction with 9 steps

1.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 1.5 h / 55 °C

1.2: 5.5 h / 0 - 55 °C

2.1: potassium carbonate / methanol / 5 h / 20 °C

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

5.1: pyridine; dmap / 2.5 h / 20 °C

6.1: lithium iodide; ammonium cerium (IV) nitrate / acetonitrile / 3 h / 85 °C

7.1: bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 7 h / 85 °C

7.2: 12 h / 20 °C

8.1: pyridine; dmap / 3 h / 20 °C

9.1: 1H-imidazole / N,N-dimethyl-formamide / 20 h / 20 °C

With pyridine; 1H-imidazole; dmap; bis-triphenylphosphine-palladium(II) chloride; N,O-bis-(trimethylsilyl)-acetamide; ammonium cerium (IV) nitrate; tetrabutyl ammonium fluoride; water; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium iodide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1174917-60-2
C₄₀H₄₄N₂O₁₀SSi

: 1314716-27-2
C₄₀H₄₅N₃O₈SSi

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate / methanol / 5 h / 20 °C

2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 20 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

4.1: pyridine; dmap / 2.5 h / 20 °C

5.1: lithium iodide; ammonium cerium (IV) nitrate / acetonitrile / 3 h / 85 °C

6.1: bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 7 h / 85 °C

6.2: 12 h / 20 °C

7.1: pyridine; dmap / 3 h / 20 °C

8.1: 1H-imidazole / N,N-dimethyl-formamide / 20 h / 20 °C

With pyridine; 1H-imidazole; dmap; bis-triphenylphosphine-palladium(II) chloride; ammonium cerium (IV) nitrate; tetrabutyl ammonium fluoride; water; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium iodide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;