C₃₄H₃₄N₂O₃

Base Information

Chemical Name:C₃₄H₃₄N₂O₃
CAS No.:247061-41-2
Molecular Formula:C₃₄H₃₄N₂O₃
Molecular Weight:518.656
Hs Code.:

C<sub>34</sub>H<sub>34</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₃₄H₃₄N₂O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₄H₃₄N₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of C₃₄H₃₄N₂O₃

There total 10 articles about C₃₄H₃₄N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 247061-40-1
(3S,3'S)-1,1'-dibenzyl-3,3'-bis-(2-hydroxyethyl)-[3,3'-biindoline]-2,2'-dione

: 247061-41-2
C₃₄H₃₄N₂O₃

Guidance literature:: With sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; Heating;
DOI:10.1021/ja991714g

Reference yield:

: 615-43-0
2-iodophenylamine

: 247061-41-2
C₃₄H₃₄N₂O₃

Guidance literature:: Multi-step reaction with 10 steps

1: 92 percent / Me₃Al / toluene / 20 °C

2: 87 percent / NaH / dimethylformamide

3: 70 percent / BCl₃ / -78 °C

4: 80 percent / camphorsulfonic acid monohydrate

5: 90 percent / (Ph₃P)2PdCl₂; Et₃N / N,N-dimethyl-acetamide / 100 °C

6: camphorsulfonic acid monohydrate / tetrahydrofuran

7: NaBH₄ / methanol

8: Pb(OAc)4 / benzene

9: NaBH₄ / methanol

10: sodium bis(2-methoxyethoxy)aluminum hydride / tetrahydrofuran / Heating

With lead(IV) acetate; bis-triphenylphosphine-palladium(II) chloride; sodium tetrahydroborate; camphor-10-sulfonic acid; trimethylaluminum; boron trichloride; sodium hydride; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; methanol; N,N-dimethyl acetamide; N,N-dimethyl-formamide; toluene; benzene; 1: Condensation / 2: N-benzylation / 3: debenzylation / 4: Condensation / 5: Cyclization / 6: Hydrolysis / 7: Reduction / 8: Ring cleavage / 9: Reduction / 10: Reduction;
DOI:10.1021/ja991714g

Reference yield:

: 371252-55-0
2,2'-((3S,3'S)-1,1'-dibenzyl-2,2'-dioxo-[3,3'-biindoline]-3,3'-diyl)diacetaldehyde

: 247061-41-2
C₃₄H₃₄N₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol

2: sodium bis(2-methoxyethoxy)aluminum hydride / tetrahydrofuran / Heating

With sodium tetrahydroborate; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; methanol; 1: Reduction / 2: Reduction;
DOI:10.1021/ja991714g