(2-chloro-4-nitrophenyl) 6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

Base Information

Chemical Name:(2-chloro-4-nitrophenyl) 6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside
CAS No.:1397274-86-0
Molecular Formula:C₂₈H₃₂ClNO₈Si
Molecular Weight:574.102
Hs Code.:

Synonyms:(2-chloro-4-nitrophenyl) 6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

Suppliers and Price of (2-chloro-4-nitrophenyl) 6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-chloro-4-nitrophenyl) 6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

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Technology Process of (2-chloro-4-nitrophenyl) 6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

There total 4 articles about (2-chloro-4-nitrophenyl) 6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 120221-14-9,119047-14-2
(2-chloro-4-nitrophenyl)-β-D-glucopyranoside

: 1397274-86-0
(2-chloro-4-nitrophenyl) 6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1021/ol3023374

Reference yield:

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 1397274-86-0
(2-chloro-4-nitrophenyl) 6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrabutylammomium bromide; sodium hydroxide / dichloromethane / 18 h / 20 °C

2.1: sodium methylate / methanol / 18 h / 20 °C

2.2: Amberlite IR-120 (H+ form)

3.1: 1H-imidazole / N,N-dimethyl-formamide / 48 h / 20 °C

With 1H-imidazole; tetrabutylammomium bromide; sodium methylate; sodium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol3023374

Reference yield:

: 619-08-9
2-chloro-4-nitrophenol

: 1397274-86-0
(2-chloro-4-nitrophenyl) 6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrabutylammomium bromide; sodium hydroxide / dichloromethane / 18 h / 20 °C

2.1: sodium methylate / methanol / 18 h / 20 °C

2.2: Amberlite IR-120 (H+ form)

3.1: 1H-imidazole / N,N-dimethyl-formamide / 48 h / 20 °C

With 1H-imidazole; tetrabutylammomium bromide; sodium methylate; sodium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol3023374