methyl 4-[([3-(9-anthryl)propyl]{2-[(tert-butoxycarbonyl)(methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate

Base Information

Chemical Name:methyl 4-[([3-(9-anthryl)propyl]{2-[(tert-butoxycarbonyl)(methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate
CAS No.:330798-31-7
Molecular Formula:C₃₃H₃₇N₃O₈S
Molecular Weight:635.738
Hs Code.:

Synonyms:methyl 4-[([3-(9-anthryl)propyl]{2-[(tert-butoxycarbonyl)(methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate

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Chemical Property of methyl 4-[([3-(9-anthryl)propyl]{2-[(tert-butoxycarbonyl)(methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate

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Technology Process of methyl 4-[([3-(9-anthryl)propyl]{2-[(tert-butoxycarbonyl)(methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate

There total 4 articles about methyl 4-[([3-(9-anthryl)propyl]{2-[(tert-butoxycarbonyl)(methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 22756-32-7
3-(9-anthracenyl)propyl bromide

: 330798-29-3
methyl 4-[({2-[(tert-butoxycarbonyl)(methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate

: 330798-31-7
methyl 4-[([3-(9-anthryl)propyl]{2-[(tert-butoxycarbonyl)(methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate

Guidance literature:: With PS-BEMP; In N,N-dimethyl-formamide; at 20 ℃; for 14h;
DOI:10.1021/ol006751n

Reference yield:

: 22689-05-0
ω-(anthracene-9-yl)propanol

: 330798-31-7
methyl 4-[([3-(9-anthryl)propyl]{2-[(tert-butoxycarbonyl)(methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / triphenylphospine dibromide; pyridine / acetonitrile / 20 h / 20 °C

2: 98 percent / PS-BEMP / dimethylformamide / 14 h / 20 °C

With pyridine; PS-BEMP; triphenylphosphine dibromide 1:1 addition complex; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol006751n

Reference yield:

: 121492-06-6
(2-aminoethyl)methylcarbamic acid tert-butyl ester

: 330798-31-7
methyl 4-[([3-(9-anthryl)propyl]{2-[(tert-butoxycarbonyl)(methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / diisopropylamine / CH₂Cl₂ / 16 h / 20 °C

2: 98 percent / PS-BEMP / dimethylformamide / 14 h / 20 °C

With PS-BEMP; diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol006751n