N,N-di-isopropyl-2-(4-benzyloxyphenyl)-3,4-dihydroxy-5-phenylpenta-2,4-dien-1-oic acid amide

Base Information

Chemical Name:N,N-di-isopropyl-2-(4-benzyloxyphenyl)-3,4-dihydroxy-5-phenylpenta-2,4-dien-1-oic acid amide
CAS No.:93831-26-6
Molecular Formula:C₃₀H₃₃NO₄
Molecular Weight:471.596
Hs Code.:

Synonyms:N,N-di-isopropyl-2-(4-benzyloxyphenyl)-3,4-dihydroxy-5-phenylpenta-2,4-dien-1-oic acid amide

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Chemical Property of N,N-di-isopropyl-2-(4-benzyloxyphenyl)-3,4-dihydroxy-5-phenylpenta-2,4-dien-1-oic acid amide

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Technology Process of N,N-di-isopropyl-2-(4-benzyloxyphenyl)-3,4-dihydroxy-5-phenylpenta-2,4-dien-1-oic acid amide

There total 3 articles about N,N-di-isopropyl-2-(4-benzyloxyphenyl)-3,4-dihydroxy-5-phenylpenta-2,4-dien-1-oic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68641-16-7
(4-benzyloxy-phenyl)-acetic acid methyl ester

: 93831-17-5
(Z)-5'-benzylidenecyclohexanespiro-2'-(1',3'-dioxolan)-4'-one

: 108-18-9
diisopropylamine

: 6547-53-1
2-[4-(benzyloxy)benzyl]acetic acid

: 93831-21-1
4-benzyloxypulvinone

: 93831-26-6
N,N-di-isopropyl-2-(4-benzyloxyphenyl)-3,4-dihydroxy-5-phenylpenta-2,4-dien-1-oic acid amide

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, -78 deg C, 25 min, 2.) -78 deg C --> room temperature, overnight;

Reference yield:

: 6547-53-1
2-[4-(benzyloxy)benzyl]acetic acid

: 93831-26-6
N,N-di-isopropyl-2-(4-benzyloxyphenyl)-3,4-dihydroxy-5-phenylpenta-2,4-dien-1-oic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / diethyl ether / Ambient temperature

2: 1.) lithium di-isopropylamide / 1.) THF, -78 deg C, 25 min, 2.) -78 deg C --> room temperature, overnight

With lithium diisopropyl amide; In diethyl ether;

Reference yield:

: 68641-16-7
(4-benzyloxy-phenyl)-acetic acid methyl ester

: 93831-17-5
(Z)-5'-benzylidenecyclohexanespiro-2'-(1',3'-dioxolan)-4'-one

: 93831-21-1
4-benzyloxypulvinone

: 93831-26-6
N,N-di-isopropyl-2-(4-benzyloxyphenyl)-3,4-dihydroxy-5-phenylpenta-2,4-dien-1-oic acid amide

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, -78 deg C, 25 min, 2.) -78 deg C --> room temperature, overnight;