Benzyl-2-acetamido-4-O-(6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl)-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

Base Information

Chemical Name:Benzyl-2-acetamido-4-O-(6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl)-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid
CAS No.:76909-88-1
Molecular Formula:C₅₆H₅₉NO₁₂
Molecular Weight:938.084
Hs Code.:

Synonyms:Benzyl-2-acetamido-4-O-(6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl)-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

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Chemical Property of Benzyl-2-acetamido-4-O-(6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl)-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

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Technology Process of Benzyl-2-acetamido-4-O-(6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl)-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

There total 4 articles about Benzyl-2-acetamido-4-O-(6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl)-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 613-90-1
benzoyl cyanide

: 76909-80-3
Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(2,3-di-O-benzyl-β-D-galactopyranosyl)-α-D-glucopyranosid

: 76909-88-1
Benzyl-2-acetamido-4-O-(6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl)-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

Guidance literature:: In pyridine; dichloromethane; at 0 ℃; for 72h;

Reference yield:

: 70209-55-1
benzyl 2-acetamido-3,6-di-O-benzyl-4-O-(4,6-O-benzylidene-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranoside

: 76909-88-1
Benzyl-2-acetamido-4-O-(6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl)-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / KOH / dimethylformamide / 3 h / 0 °C

2: 89 percent / 90percent CH₃COOH / 2.5 h / 60 °C

3: 92 percent / CH₂Cl₂; pyridine / 72 h / 0 °C

With potassium hydroxide; acetic acid; In pyridine; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 100-39-0
benzyl bromide

: 76909-88-1
Benzyl-2-acetamido-4-O-(6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl)-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / KOH / dimethylformamide / 3 h / 0 °C

2: 89 percent / 90percent CH₃COOH / 2.5 h / 60 °C

3: 92 percent / CH₂Cl₂; pyridine / 72 h / 0 °C

With potassium hydroxide; acetic acid; In pyridine; dichloromethane; N,N-dimethyl-formamide;