phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-4-deoxy-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-4-deoxy-1-thio-β-D-glucopyranoside
CAS No.:1319721-56-6
Molecular Formula:C₄₂H₄₂O₆SSi
Molecular Weight:702.943
Hs Code.:

Synonyms:phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-4-deoxy-1-thio-β-D-glucopyranoside

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Chemical Property of phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-4-deoxy-1-thio-β-D-glucopyranoside

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Technology Process of phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-4-deoxy-1-thio-β-D-glucopyranoside

There total 4 articles about phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-4-deoxy-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1319721-74-8
C₄₆H₄₄N₂O₇S₂Si

: 1319721-56-6
phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-4-deoxy-1-thio-β-D-glucopyranoside

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 90 ℃; for 2h;
DOI:10.1016/j.carres.2011.03.042

Reference yield:

: 1319721-55-5
phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-1-thio-β-D-glucopyranoside

: 1319721-56-6
phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-4-deoxy-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 5 h / 90 °C

2: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / 90 °C

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene;
DOI:10.1016/j.carres.2011.03.042

Reference yield:

: 138857-50-8
phenyl 2,3-bis-O-benzoyl-1-thio-β-D-glucopyranoside

: 1319721-56-6
phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-4-deoxy-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 20 h

2: toluene / 5 h / 90 °C

3: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / 90 °C

With 1H-imidazole; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.carres.2011.03.042