(2Z)-2-[1-(2-bromo-5-chlorophenyl)-2-(2,3,6-trifluorophenyl)ethylidene]hydrazinecarboximidamide

Base Information

Chemical Name:(2Z)-2-[1-(2-bromo-5-chlorophenyl)-2-(2,3,6-trifluorophenyl)ethylidene]hydrazinecarboximidamide
CAS No.:1350855-85-4
Molecular Formula:C₁₅H₁₁BrClF₃N₄
Molecular Weight:419.631
Hs Code.:

Synonyms:(2Z)-2-[1-(2-bromo-5-chlorophenyl)-2-(2,3,6-trifluorophenyl)ethylidene]hydrazinecarboximidamide

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Chemical Property of (2Z)-2-[1-(2-bromo-5-chlorophenyl)-2-(2,3,6-trifluorophenyl)ethylidene]hydrazinecarboximidamide

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Technology Process of (2Z)-2-[1-(2-bromo-5-chlorophenyl)-2-(2,3,6-trifluorophenyl)ethylidene]hydrazinecarboximidamide

There total 3 articles about (2Z)-2-[1-(2-bromo-5-chlorophenyl)-2-(2,3,6-trifluorophenyl)ethylidene]hydrazinecarboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1228788-17-7
1-(2-bromo-5-chlorophenyl)-2-(2,3,6-trifluorophenyl)ethanone

: 1937-19-5,16139-18-7
1-aminoguanidine hydrochloride

: 1350855-85-4
(2Z)-2-[1-(2-bromo-5-chlorophenyl)-2-(2,3,6-trifluorophenyl)ethylidene]hydrazinecarboximidamide

Guidance literature:: 1-(2-bromo-5-chlorophenyl)-2-(2,3,6-trifluorophenyl)ethanone; 1-aminoguanidine hydrochloride; With boron trifluoride diethyl etherate; In methanol; at 100 ℃; for 4h; Inert atmosphere;

With sodium hydroxide; In water; ethyl acetate;

Reference yield:

: 114152-23-7
2-(2,3,6-trifluorophenyl)acetic acid

: 1350855-85-4
(2Z)-2-[1-(2-bromo-5-chlorophenyl)-2-(2,3,6-trifluorophenyl)ethylidene]hydrazinecarboximidamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hexamethyldisilazane / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / methanol / 4 h / 100 °C / Inert atmosphere

With boron trifluoride diethyl etherate; sodium hexamethyldisilazane; In tetrahydrofuran; methanol;

Reference yield:

: 27007-53-0
methyl-2-bromo-5-chlorobenzoate

: 1350855-85-4
(2Z)-2-[1-(2-bromo-5-chlorophenyl)-2-(2,3,6-trifluorophenyl)ethylidene]hydrazinecarboximidamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hexamethyldisilazane / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / methanol / 4 h / 100 °C / Inert atmosphere

With boron trifluoride diethyl etherate; sodium hexamethyldisilazane; In tetrahydrofuran; methanol;