methyl (S)-(3-(N-phenyl-N-2-pyridyl)amino)-2-(di-tert-butoxycarbonylamino)-propionate

Base Information

Chemical Name:methyl (S)-(3-(N-phenyl-N-2-pyridyl)amino)-2-(di-tert-butoxycarbonylamino)-propionate
CAS No.:869796-52-1
Molecular Formula:C₂₅H₃₃N₃O₆
Molecular Weight:471.554
Hs Code.:

Synonyms:methyl (S)-(3-(N-phenyl-N-2-pyridyl)amino)-2-(di-tert-butoxycarbonylamino)-propionate

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Chemical Property of methyl (S)-(3-(N-phenyl-N-2-pyridyl)amino)-2-(di-tert-butoxycarbonylamino)-propionate

Chemical Property:

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Technology Process of methyl (S)-(3-(N-phenyl-N-2-pyridyl)amino)-2-(di-tert-butoxycarbonylamino)-propionate

There total 4 articles about methyl (S)-(3-(N-phenyl-N-2-pyridyl)amino)-2-(di-tert-butoxycarbonylamino)-propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 673488-57-8
(3-(N-phenyl-N-pyridin-2-yl)-amino)-2-(di-tert-butoxycarbonyl)-amino-propionic acid methyl ester

: 869796-52-1
methyl (S)-(3-(N-phenyl-N-2-pyridyl)amino)-2-(di-tert-butoxycarbonylamino)-propionate

: methyl (R)-(3-(N-phenyl-N-2-pyridyl)amino)-2-(di-tert-butoxycarbonylamino)-propionate

Guidance literature:: at 20 ℃; Purification / work up; Resolution of racemate;

Reference yield:

: 201338-62-7
N,N-tert-butoxycarbonyldehydroalanine

: 869796-52-1
methyl (S)-(3-(N-phenyl-N-2-pyridyl)amino)-2-(di-tert-butoxycarbonylamino)-propionate

: methyl (R)-(3-(N-phenyl-N-2-pyridyl)amino)-2-(di-tert-butoxycarbonylamino)-propionate

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / acetonitrile / 48 h / 45 °C

2: Resolution of racemate

With caesium carbonate; In acetonitrile;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 869796-52-1
methyl (S)-(3-(N-phenyl-N-2-pyridyl)amino)-2-(di-tert-butoxycarbonylamino)-propionate

: methyl (R)-(3-(N-phenyl-N-2-pyridyl)amino)-2-(di-tert-butoxycarbonylamino)-propionate

Guidance literature:: Multi-step reaction with 3 steps

1: dmap / acetonitrile / 8 h / 22 - 50 °C

2: caesium carbonate / acetonitrile / 48 h / 45 °C

3: Resolution of racemate

With dmap; caesium carbonate; In acetonitrile;