1-cyclohexyl-2-methyl-cyclopentene

Base Information

• Chemical Name: 1-cyclohexyl-2-methyl-cyclopentene
• CAS No.: 858423-14-0
• Molecular Formula: C₁₂H₂₀
• Molecular Weight: 164.291
• Mol file: 858423-14-0.mol

Synonyms:1-cyclohexyl-2-methyl-cyclopentene

Chemical Property of 1-cyclohexyl-2-methyl-cyclopentene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-cyclohexyl-2-methyl-cyclopentene

There total 6 articles about 1-cyclohexyl-2-methyl-cyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexylmagnesium bromide (931-50-0) → 1-cyclohexyl-2-methyl-cyclopentene (858423-14-0)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: KHSO₄ / 180 - 190 °C

With potassium hydrogensulfate; diethyl ether;

Reference yield:

optically inactive 2-hydroxy-1-methyl-2-cyclohexyl-cyclopentane (859181-97-8) → 1-cyclohexyl-2-methyl-cyclopentene (858423-14-0)

Guidance literature:

With potassium hydrogensulfate; at 180 - 190 ℃;

Reference yield:

2-Methylcyclopentanone (1120-72-5) + cyclohexylmagnesiumchloride (931-51-1) → 1-cyclohexyl-2-methyl-cyclopentene (858423-14-0)

Guidance literature:

With diethyl ether; at -40 ℃; Erhitzen des nach dem Ansaeuern erhaltenen Reaktionsprodukts mit Kaliumhydrogensulfat unter 120 Torr auf 160grad;

upstream raw materials:

2-Methylcyclopentanone

cyclohexylmagnesiumchloride

1-cyclohexyl-bicyclo[3.1.0]hexane

optically inactive 2-hydroxy-1-methyl-2-cyclohexyl-cyclopentane

Downstream raw materials:

1-cyclohexyl-hexane-1,5-dione

3-(cyclohexylidene)cyclohexene

[1,1'-bi(cyclohexan)]-1-en-3-one