3-(2-chloro-ethoxy)-N-(3,5-dichloro-pyridin-4-yl)-4-methoxy-benzamide

Base Information

Chemical Name:3-(2-chloro-ethoxy)-N-(3,5-dichloro-pyridin-4-yl)-4-methoxy-benzamide
CAS No.:1176169-45-1
Molecular Formula:C₁₅H₁₃Cl₃N₂O₃
Molecular Weight:375.639
Hs Code.:

Synonyms:3-(2-chloro-ethoxy)-N-(3,5-dichloro-pyridin-4-yl)-4-methoxy-benzamide

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Chemical Property of 3-(2-chloro-ethoxy)-N-(3,5-dichloro-pyridin-4-yl)-4-methoxy-benzamide

Chemical Property:

Purity/Quality:

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Technology Process of 3-(2-chloro-ethoxy)-N-(3,5-dichloro-pyridin-4-yl)-4-methoxy-benzamide

There total 2 articles about 3-(2-chloro-ethoxy)-N-(3,5-dichloro-pyridin-4-yl)-4-methoxy-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22889-78-7
3,5-dichloro-4-aminopyridine

: 1176169-43-9
C₁₀H₁₁ClO₄

: 1176169-45-1
3-(2-chloro-ethoxy)-N-(3,5-dichloro-pyridin-4-yl)-4-methoxy-benzamide

Guidance literature:: 3,5-dichloro-4-aminopyridine; With sodium hydride; In N,N-dimethyl-formamide; at 28 ℃; for 3h;

C₁₀H₁₁ClO₄; With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 0 - 10 ℃;

Reference yield:

: 645-08-9,74309-78-7
Isovanillic acid

: 1176169-45-1
3-(2-chloro-ethoxy)-N-(3,5-dichloro-pyridin-4-yl)-4-methoxy-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 7 h / 50 - 70 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 3 h / 28 °C

2.2: 0 - 10 °C

With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide;

Reference yield:

: 1176169-45-1
3-(2-chloro-ethoxy)-N-(3,5-dichloro-pyridin-4-yl)-4-methoxy-benzamide

: 1185160-57-9
C₄₆H₇₅NO₁₆S₂

: 1185160-61-5
C₆₀H₈₅Cl₂N₃O₁₉S

Guidance literature:: C₄₆H₇₅NO₁₆S₂; With tributylphosphine; water; In N,N-dimethyl-formamide; at 0 - 5 ℃; for 1h; Inert atmosphere;

3-(2-chloro-ethoxy)-N-(3,5-dichloro-pyridin-4-yl)-4-methoxy-benzamide; With 1,8-diazabicyclo[5.4.0]undec-7-ene; potassium iodide; In N,N-dimethyl-formamide; at 20 ℃; for 12h; Inert atmosphere;