4-cyanophenyl methyl phosphonochloridothioate

Base Information

• Chemical Name: 4-cyanophenyl methyl phosphonochloridothioate
• CAS No.: 1186024-70-3
• Molecular Formula: C₈H₇ClNOPS
• Molecular Weight: 231.642

Synonyms:4-cyanophenyl methyl phosphonochloridothioate

Chemical Property of 4-cyanophenyl methyl phosphonochloridothioate

Chemical Property:

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Technology Process of 4-cyanophenyl methyl phosphonochloridothioate

There total 1 articles about 4-cyanophenyl methyl phosphonochloridothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-cyanophenol (767-00-0) + methylphosphonothioic dichloride (676-98-2) → 4-cyanophenyl methyl phosphonochloridothioate (1186024-70-3)

Guidance literature:

With triethylamine; In dichloromethane; for 2h; Cooling with ice;

DOI:10.1039/b903148k

Reference yield:

4-cyanophenyl methyl phosphonochloridothioate (1186024-70-3) + p-toluidine (106-49-0,12221-03-3) → C15H15N2OPS + p-toluidine hydrochloride (540-23-8)

Guidance literature:

In acetonitrile; at 55 ℃; Kinetics; Mechanism;

DOI:10.1039/b903148k

Reference yield:

4-cyanophenyl methyl phosphonochloridothioate (1186024-70-3) + 3-nitro-aniline (99-09-2) → C14H12N3O3PS + 3-nitroaniline hydrochloride (33240-96-9)

Guidance literature:

In acetonitrile; at 55 ℃; Kinetics; Mechanism;

DOI:10.1039/b903148k

upstream raw materials:

4-cyanophenol

methylphosphonothioic dichloride

Downstream raw materials:

p-toluidine hydrochloride

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