carbonic acid ethyl 2-(1-methoxypiperidin-4-yl)-5-oxo-4-(2,4,6-trimethylphenyl)-2,5-dihydro-1H-pyrrol-3-yl ester

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Chemical Name:carbonic acid ethyl 2-(1-methoxypiperidin-4-yl)-5-oxo-4-(2,4,6-trimethylphenyl)-2,5-dihydro-1H-pyrrol-3-yl ester
CAS No.:1384930-00-0
Molecular Formula:C₂₂H₃₀N₂O₅
Molecular Weight:402.491
Hs Code.:

Synonyms:carbonic acid ethyl 2-(1-methoxypiperidin-4-yl)-5-oxo-4-(2,4,6-trimethylphenyl)-2,5-dihydro-1H-pyrrol-3-yl ester

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Chemical Property of carbonic acid ethyl 2-(1-methoxypiperidin-4-yl)-5-oxo-4-(2,4,6-trimethylphenyl)-2,5-dihydro-1H-pyrrol-3-yl ester

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Technology Process of carbonic acid ethyl 2-(1-methoxypiperidin-4-yl)-5-oxo-4-(2,4,6-trimethylphenyl)-2,5-dihydro-1H-pyrrol-3-yl ester

There total 7 articles about carbonic acid ethyl 2-(1-methoxypiperidin-4-yl)-5-oxo-4-(2,4,6-trimethylphenyl)-2,5-dihydro-1H-pyrrol-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-hydroxy-5-(1-methoxypiperidin-4-yl)-3-(2,4,6-trimethylphenyl)-1,5-dihydro-pyrrol-2-one

: 541-41-3
chloroformic acid ethyl ester

: 1384930-00-0
carbonic acid ethyl 2-(1-methoxypiperidin-4-yl)-5-oxo-4-(2,4,6-trimethylphenyl)-2,5-dihydro-1H-pyrrol-3-yl ester

Guidance literature:: With dmap; triethylamine; In acetone; for 0.25h;

Reference yield:

: 1384930-71-5
1-methoxy-4-methoxymethylenepiperidine

: 1384930-00-0
carbonic acid ethyl 2-(1-methoxypiperidin-4-yl)-5-oxo-4-(2,4,6-trimethylphenyl)-2,5-dihydro-1H-pyrrol-3-yl ester

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogenchloride; water / tetrahydrofuran / 4 h / 20 °C

2: ammonia; ammonium chloride / water / 12 h / 20 °C

3: triethylamine / tetrahydrofuran / 0.5 h / 20 °C

4: hydrogenchloride / methanol / 12 h / Reflux

5: potassium tert-butylate / N,N-dimethyl-formamide / 0.17 h / 90 °C / Inert atmosphere

6: dmap; triethylamine / acetone / 0.25 h

With hydrogenchloride; dmap; potassium tert-butylate; ammonia; water; ammonium chloride; triethylamine; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 1384930-58-8
amino-(1-methoxypiperidin-4-yl)acetonitrile

: 1384930-00-0
carbonic acid ethyl 2-(1-methoxypiperidin-4-yl)-5-oxo-4-(2,4,6-trimethylphenyl)-2,5-dihydro-1H-pyrrol-3-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / tetrahydrofuran / 0.5 h / 20 °C

2: hydrogenchloride / methanol / 12 h / Reflux

3: potassium tert-butylate / N,N-dimethyl-formamide / 0.17 h / 90 °C / Inert atmosphere

4: dmap; triethylamine / acetone / 0.25 h

With hydrogenchloride; dmap; potassium tert-butylate; triethylamine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetone;