1-[[4-(1,1-dimethylethyl)phenyl]sulfonyl]-1,2,3,4-tetrahydro-2-quinolinylcarboxylic acid methyl ester

Base Information

Chemical Name:1-[[4-(1,1-dimethylethyl)phenyl]sulfonyl]-1,2,3,4-tetrahydro-2-quinolinylcarboxylic acid methyl ester
CAS No.:869059-52-9
Molecular Formula:C₂₁H₂₅NO₄S
Molecular Weight:387.5
Hs Code.:

Synonyms:1-[[4-(1,1-dimethylethyl)phenyl]sulfonyl]-1,2,3,4-tetrahydro-2-quinolinylcarboxylic acid methyl ester

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Chemical Property of 1-[[4-(1,1-dimethylethyl)phenyl]sulfonyl]-1,2,3,4-tetrahydro-2-quinolinylcarboxylic acid methyl ester

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Technology Process of 1-[[4-(1,1-dimethylethyl)phenyl]sulfonyl]-1,2,3,4-tetrahydro-2-quinolinylcarboxylic acid methyl ester

There total 1 articles about 1-[[4-(1,1-dimethylethyl)phenyl]sulfonyl]-1,2,3,4-tetrahydro-2-quinolinylcarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 15084-51-2
4-tert-butylbenzenesulfonyl chloride

: 63430-79-5
1,2,3,4-tetrahydro-quinoline-2-carboxylic acid methyl ester

: 869059-52-9
1-[[4-(1,1-dimethylethyl)phenyl]sulfonyl]-1,2,3,4-tetrahydro-2-quinolinylcarboxylic acid methyl ester

Guidance literature:: With 4-methyl-morpholine; In acetonitrile; for 18h; Heating / reflux;

Reference yield: 86.0%

: 869059-52-9
1-[[4-(1,1-dimethylethyl)phenyl]sulfonyl]-1,2,3,4-tetrahydro-2-quinolinylcarboxylic acid methyl ester

: 869059-53-0
1-[[4-(1,1-dimethylethyl)phenyl]sulfonyl]-1,2,3,4-tetrahydro-2-quinolinylcarboxylic acid

Guidance literature:: 1-[[4-(1,1-dimethylethyl)phenyl]sulfonyl]-1,2,3,4-tetrahydro-2-quinolinylcarboxylic acid methyl ester; With lithium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 2h;

With hydrogenchloride; In tetrahydrofuran; water; pH=1;