ethyl 3-({[(4-hydroxy-3,5-di-tert-butylphenyl)acetyl]amino}sulfonyl)-4-chlorobenzoate

Base Information

Chemical Name:ethyl 3-({[(4-hydroxy-3,5-di-tert-butylphenyl)acetyl]amino}sulfonyl)-4-chlorobenzoate
CAS No.:190833-89-7
Molecular Formula:C₂₅H₃₂ClNO₆S
Molecular Weight:510.051
Hs Code.:

Synonyms:ethyl 3-({[(4-hydroxy-3,5-di-tert-butylphenyl)acetyl]amino}sulfonyl)-4-chlorobenzoate

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Chemical Property of ethyl 3-({[(4-hydroxy-3,5-di-tert-butylphenyl)acetyl]amino}sulfonyl)-4-chlorobenzoate

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Technology Process of ethyl 3-({[(4-hydroxy-3,5-di-tert-butylphenyl)acetyl]amino}sulfonyl)-4-chlorobenzoate

There total 1 articles about ethyl 3-({[(4-hydroxy-3,5-di-tert-butylphenyl)acetyl]amino}sulfonyl)-4-chlorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 156-38-7
4-hydroxyphenylacetate

: 190833-89-7
ethyl 3-({[(4-hydroxy-3,5-di-tert-butylphenyl)acetyl]amino}sulfonyl)-4-chlorobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / 70percent aq. HClO₄

2: DMAP, DCC / dimethylformamide / 48 h / Ambient temperature

With dmap; perchloric acid; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1021/jm960772z

Reference yield:

: 190833-89-7
ethyl 3-({[(4-hydroxy-3,5-di-tert-butylphenyl)acetyl]amino}sulfonyl)-4-chlorobenzoate

: 190833-93-3
3-({[(4-hydroxy-3,5-di-tert-butylphenyl)acetyl]amino}sulfonyl)-4-chlorobenzoic acid

Guidance literature:: With sodium hydroxide; In ethanol; at 60 ℃; for 20h;
DOI:10.1021/jm960772z

Reference yield:

: 190833-89-7
ethyl 3-({[(4-hydroxy-3,5-di-tert-butylphenyl)acetyl]amino}sulfonyl)-4-chlorobenzoate

: 161787-52-6
4-[({[4-chloro-3-({[(4-hydroxy-3,5-di-tert-butylphenyl)acetyl]amino}sulfonyl)phenyl]carbonyl}amino)sulfonyl]benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: aq. NaOH / ethanol / 20 h / 60 °C

2: DCC, DMAP / dimethylformamide / 2 h / Ambient temperature

3: aq. NaOH / ethanol / 20 h / 60 °C

With dmap; sodium hydroxide; dicyclohexyl-carbodiimide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm960772z