[2-(tert-Butyl-dimethyl-silanyloxy)-phenyl]-carbamic acid 6-(tert-butyl-dimethyl-silanyloxymethyl)-[1,2]dithiin-3-ylmethyl ester

Base Information

Chemical Name:[2-(tert-Butyl-dimethyl-silanyloxy)-phenyl]-carbamic acid 6-(tert-butyl-dimethyl-silanyloxymethyl)-[1,2]dithiin-3-ylmethyl ester
CAS No.:165404-66-0
Molecular Formula:C₂₅H₄₁NO₄S₂Si₂
Molecular Weight:539.908
Hs Code.:

Synonyms:[2-(tert-Butyl-dimethyl-silanyloxy)-phenyl]-carbamic acid 6-(tert-butyl-dimethyl-silanyloxymethyl)-[1,2]dithiin-3-ylmethyl ester

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Chemical Property of [2-(tert-Butyl-dimethyl-silanyloxy)-phenyl]-carbamic acid 6-(tert-butyl-dimethyl-silanyloxymethyl)-[1,2]dithiin-3-ylmethyl ester

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Technology Process of [2-(tert-Butyl-dimethyl-silanyloxy)-phenyl]-carbamic acid 6-(tert-butyl-dimethyl-silanyloxymethyl)-[1,2]dithiin-3-ylmethyl ester

There total 7 articles about [2-(tert-Butyl-dimethyl-silanyloxy)-phenyl]-carbamic acid 6-(tert-butyl-dimethyl-silanyloxymethyl)-[1,2]dithiin-3-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 165405-44-7
2-(tert-butyldimethylsilanyloxy)phenyl isocyanate

: 165404-83-1
3-[(tert-butyldimethylsilyloxy)methyl]-6-(hydroxymethyl)-1,2-dithiin

: 165404-66-0
[2-(tert-Butyl-dimethyl-silanyloxy)-phenyl]-carbamic acid 6-(tert-butyl-dimethyl-silanyloxymethyl)-[1,2]dithiin-3-ylmethyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; for 15h; Ambient temperature;
DOI:10.1021/jm00014a016

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 165404-66-0
[2-(tert-Butyl-dimethyl-silanyloxy)-phenyl]-carbamic acid 6-(tert-butyl-dimethyl-silanyloxymethyl)-[1,2]dithiin-3-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / 15 h / Ambient temperature

2: Et₃N / toluene / 1 h / Ambient temperature

3: 87 percent / Et₃N / tetrahydrofuran / 15 h / Ambient temperature

With triethylamine; In tetrahydrofuran; toluene;
DOI:10.1021/jm00014a016

Reference yield:

: 69589-21-5
O-tert-butyldimethylsilyl-2-aminophenol

: 165404-66-0
[2-(tert-Butyl-dimethyl-silanyloxy)-phenyl]-carbamic acid 6-(tert-butyl-dimethyl-silanyloxymethyl)-[1,2]dithiin-3-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / toluene / 1 h / Ambient temperature

2: 87 percent / Et₃N / tetrahydrofuran / 15 h / Ambient temperature

With triethylamine; In tetrahydrofuran; toluene;
DOI:10.1021/jm00014a016