2-Bromocyclohexanonoxim

Base Information

• Chemical Name: 2-Bromocyclohexanonoxim
• CAS No.: 70224-65-6
• Molecular Formula: C₆H₁₀BrNO
• Molecular Weight: 192.055
• Mol file: 70224-65-6.mol

Synonyms:2-Bromocyclohexanonoxim

Chemical Property of 2-Bromocyclohexanonoxim

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Bromocyclohexanonoxim

There total 1 articles about 2-Bromocyclohexanonoxim which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromocyclohexanone (1056477-06-5,822-85-5) → 2-Bromocyclohexanonoxim (70224-65-6)

Guidance literature:

With hydroxylamine hydrochloride;

DOI:10.1016/j.tetlet.2009.10.060

Reference yield: 45.0%

2-Bromocyclohexanonoxim (70224-65-6) → 1-nitrocyclohexene (2562-37-0)

Guidance literature:

With disodium hydrogenphosphate; dihydrogen peroxide; urea; trifluoroacetic anhydride; In acetonitrile; for 0.5h; Ambient temperature;

DOI:10.1246/bcsj.55.635

Reference yield:

2-Bromocyclohexanonoxim (70224-65-6) → 1-Chloro-1-nitroso-2-bromocyclohexan (70224-66-7)

Guidance literature:

With chlorine; In dichloromethane;

DOI:10.1021/jo01328a002

upstream raw materials:

2-bromocyclohexanone

Downstream raw materials:

1-Chloro-1-nitroso-2-bromocyclohexan

1-nitrocyclohexene

N-Carbethoxy-N'-(1-chloro-2-bromocyclohexyl)-diazen-N'-oxid

Refernces