4-(6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)-N,N-diethylbenzamide

Base Information

Chemical Name:4-(6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)-N,N-diethylbenzamide
CAS No.:857252-28-9
Molecular Formula:C₂₂H₂₈N₂O₃
Molecular Weight:368.476
Hs Code.:

Synonyms:4-(6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)-N,N-diethylbenzamide

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Chemical Property of 4-(6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)-N,N-diethylbenzamide

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Technology Process of 4-(6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)-N,N-diethylbenzamide

There total 1 articles about 4-(6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)-N,N-diethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 58287-77-7
N,N-diethyl-4-formylbenzamide

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 857252-28-9
4-(6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)-N,N-diethylbenzamide

Guidance literature:: N,N-diethyl-4-formylbenzamide; 2-(3,4-dimethoxyphenyl)-ethylamine; With trifluoroacetic acid; for 18h; Heating / reflux;

With sodium hydrogencarbonate; In dichloromethane; water;

Reference yield: 100.0%

: 857252-28-9
4-(6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)-N,N-diethylbenzamide

: 68282-47-3
2-phenyl-1H-imidazole-4-carbaldehyde

: 4-{6,7-dimethoxy-2-[(2-phenyl-1H-imidazol-5-yl)methyl]-1,2,3,4-tetrahydroisoquinolin-1-yl}-N,N-diethylbenzamide

Guidance literature:: 4-(6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)-N,N-diethylbenzamide; 2-phenyl-1H-imidazole-4-carbaldehyde; In 1-methyl-pyrrolidin-2-one; 1,2-dichloro-ethane; at 20 ℃; for 0.166667h;

With sodium tris(acetoxy)borohydride; In 1-methyl-pyrrolidin-2-one; 1,2-dichloro-ethane; at 20 ℃; for 18h;