N-(2,3-dihydroxy-2-methyl-propyl)-4-methyl-N-prop-2-ynyl-benzenesulfonamide

Base Information

Chemical Name:N-(2,3-dihydroxy-2-methyl-propyl)-4-methyl-N-prop-2-ynyl-benzenesulfonamide
CAS No.:357980-48-4
Molecular Formula:C₁₄H₁₉NO₄S
Molecular Weight:297.375
Hs Code.:

<i>N</i>-(2,3-dihydroxy-2-methyl-propyl)-4-methyl-<i>N</i>-prop-2-ynyl-benzenesulfonamide

Synonyms:N-(2,3-dihydroxy-2-methyl-propyl)-4-methyl-N-prop-2-ynyl-benzenesulfonamide

Suppliers and Price of N-(2,3-dihydroxy-2-methyl-propyl)-4-methyl-N-prop-2-ynyl-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2,3-dihydroxy-2-methyl-propyl)-4-methyl-N-prop-2-ynyl-benzenesulfonamide

Chemical Property:

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Technology Process of N-(2,3-dihydroxy-2-methyl-propyl)-4-methyl-N-prop-2-ynyl-benzenesulfonamide

There total 1 articles about N-(2,3-dihydroxy-2-methyl-propyl)-4-methyl-N-prop-2-ynyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 132330-45-1
4-methyl-N-(2-methylallyl)-N-(prop-2-ynyl)benzenesulfonamide

: N-(2,3-dihydroxy-2-methyl-propyl)-4-methyl-N-prop-2-ynyl-benzenesulfonamide

: 357980-48-4
N-(2,3-dihydroxy-2-methyl-propyl)-4-methyl-N-prop-2-ynyl-benzenesulfonamide

Guidance literature:: With titanium(IV) isopropylate; AD-mix-α; tert-butyl alcohol; Title compound not separated from byproducts.;
DOI:10.1021/ja0106016

Reference yield: 78.0%

: 98-59-9
p-toluenesulfonyl chloride

: 357980-48-4
N-(2,3-dihydroxy-2-methyl-propyl)-4-methyl-N-prop-2-ynyl-benzenesulfonamide

: 503273-40-3
toluene-4-sulfonic acid 2-hydroxy-2-methyl-3-[prop-2-ynyl(toluene-4-sulfonyl)amino]propyl ester

Guidance literature:: With pyridine; for 4h;
DOI:10.1021/jo020669j

Reference yield:

: 357980-48-4
N-(2,3-dihydroxy-2-methyl-propyl)-4-methyl-N-prop-2-ynyl-benzenesulfonamide

: 4-methyl-N-(2-methyloxyranylmethyl)-N-(prop-2-ynyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / pyridine / 4 h

2: 84 percent / K₂CO₃ / methanol / 6 h

With pyridine; potassium carbonate; In methanol;
DOI:10.1021/jo020669j