(3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-(4-methoxy-benzyloxymethoxy)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

Base Information

Chemical Name:(3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-(4-methoxy-benzyloxymethoxy)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene
CAS No.:118617-83-7
Molecular Formula:C₃₆H₅₆O₃
Molecular Weight:536.839
Hs Code.:

(3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-(4-methoxy-benzyloxymethoxy)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

Synonyms:(3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-(4-methoxy-benzyloxymethoxy)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

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Chemical Property of (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-(4-methoxy-benzyloxymethoxy)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

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Technology Process of (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-(4-methoxy-benzyloxymethoxy)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

There total 3 articles about (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-(4-methoxy-benzyloxymethoxy)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 57-88-5
cholesterol

: 88023-78-3
para-methoxybenzyl chloride

: 118617-83-7
(3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-(4-methoxy-benzyloxymethoxy)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1016/S0040-4039(00)95608-9

Reference yield:

: 53942-86-2
4-methoxybenzyl alcohol sodium salt

: 118617-83-7
(3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-(4-methoxy-benzyloxymethoxy)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

Guidance literature:: Multi-step reaction with 3 steps

2: sulfuryl chloride / CH₂Cl₂ / -78 °C

3: 78 percent / diisopropylethylamine / CH₂Cl₂ / 4 h / Ambient temperature

With sulfuryl dichloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)95608-9

Reference yield:

: 88023-83-0
1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

: 118617-83-7
(3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-3-(4-methoxy-benzyloxymethoxy)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuryl chloride / CH₂Cl₂ / -78 °C

2: 78 percent / diisopropylethylamine / CH₂Cl₂ / 4 h / Ambient temperature

With sulfuryl dichloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)95608-9