1-<(trans-β-carbethoxyacryloyl)oxy>-5,5-dimethyl-3-cyclohex-2-ene

Base Information

Chemical Name:1-<(trans-β-carbethoxyacryloyl)oxy>-5,5-dimethyl-3-cyclohex-2-ene
CAS No.:84132-68-3
Molecular Formula:C₁₉H₃₀O₄Si
Molecular Weight:350.53
Hs Code.:

1-<(trans-β-carbethoxyacryloyl)oxy>-5,5-dimethyl-3-<trans-β-(trimethylsilyl)vinyl>cyclohex-2-ene

Synonyms:1-<(trans-β-carbethoxyacryloyl)oxy>-5,5-dimethyl-3-cyclohex-2-ene

Suppliers and Price of 1-<(trans-β-carbethoxyacryloyl)oxy>-5,5-dimethyl-3-cyclohex-2-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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price

Total 1 raw suppliers

Chemical Property of 1-<(trans-β-carbethoxyacryloyl)oxy>-5,5-dimethyl-3-cyclohex-2-ene

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 1-<(trans-β-carbethoxyacryloyl)oxy>-5,5-dimethyl-3-cyclohex-2-ene

There total 4 articles about 1-<(trans-β-carbethoxyacryloyl)oxy>-5,5-dimethyl-3-cyclohex-2-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 76999-38-7
5,5-dimethyl-3-cyclohex-2-en-1-ol

: 26367-48-6
fumaric acid ethyl ester mono chloride

: 84132-68-3
1-<(trans-β-carbethoxyacryloyl)oxy>-5,5-dimethyl-3-cyclohex-2-ene

Guidance literature:: In tetrahydrofuran; pyridine; at 25 ℃; for 14.5h;
DOI:10.1021/jo00152a009

Reference yield:

: 4683-45-8
3-methoxy-5,5-dimethyl-cyclohex-2-enone

: 84132-68-3
1-<(trans-β-carbethoxyacryloyl)oxy>-5,5-dimethyl-3-cyclohex-2-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / tetrahydrofuran / 1.) -78 deg C, 2.) 4,5 h, room temp.

2: 96 percent / LiAlH₄ / diethyl ether / 1.75 h / -20 °C

3: 95 percent / tetrahydrofuran; pyridine / 14.5 h / 25 °C

With lithium aluminium tetrahydride; In tetrahydrofuran; pyridine; diethyl ether;
DOI:10.1021/jo00152a009

Reference yield:

: 55339-31-6,41309-44-8
lithium

: 84132-68-3
1-<(trans-β-carbethoxyacryloyl)oxy>-5,5-dimethyl-3-cyclohex-2-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / tetrahydrofuran / 1.) -78 deg C, 2.) 4,5 h, room temp.

2: 96 percent / LiAlH₄ / diethyl ether / 1.75 h / -20 °C

3: 95 percent / tetrahydrofuran; pyridine / 14.5 h / 25 °C

With lithium aluminium tetrahydride; In tetrahydrofuran; pyridine; diethyl ether;
DOI:10.1021/jo00152a009