2,2',2'',2'''-tetrakis(phenylmethoxy)-<1,1':3'',1'':1'''-quaterphenyl>-3,3'''-dimethanol

Base Information

Chemical Name:2,2',2'',2'''-tetrakis(phenylmethoxy)-<1,1':3'',1'':1'''-quaterphenyl>-3,3'''-dimethanol
CAS No.:123291-87-2
Molecular Formula:C₅₄H₄₆O₆
Molecular Weight:790.956
Hs Code.:

Synonyms:2,2',2'',2'''-tetrakis(phenylmethoxy)-<1,1':3'',1'':1'''-quaterphenyl>-3,3'''-dimethanol

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Chemical Property of 2,2',2'',2'''-tetrakis(phenylmethoxy)-<1,1':3'',1'':1'''-quaterphenyl>-3,3'''-dimethanol

Chemical Property:

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Technology Process of 2,2',2'',2'''-tetrakis(phenylmethoxy)-<1,1':3'',1'':1'''-quaterphenyl>-3,3'''-dimethanol

There total 4 articles about 2,2',2'',2'''-tetrakis(phenylmethoxy)-<1,1':3'',1'':1'''-quaterphenyl>-3,3'''-dimethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 123291-86-1
2,2',2'',2'''-Tetrakis-benzyloxy-[1,3';1',1'';3'',1''']quaterphenyl-3,3'''-dicarboxylic acid diethyl ester

: 123291-87-2
2,2',2'',2'''-tetrakis(phenylmethoxy)-<1,1':3'',1'':1'''-quaterphenyl>-3,3'''-dimethanol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; for 0.666667h;
DOI:10.1021/jo00284a018

Reference yield:

: 100-39-0
benzyl bromide

: 123291-87-2
2,2',2'',2'''-tetrakis(phenylmethoxy)-<1,1':3'',1'':1'''-quaterphenyl>-3,3'''-dimethanol

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / acetone / 168 h / Heating

2: NaOH / ethanol; H₂O / 8 h / Heating

3: 100 percent / K₂CO₃ / acetone / 15 h / Heating

4: 87 percent / LiAlH₄ / diethyl ether / 0.67 h / 0 °C

With sodium hydroxide; lithium aluminium tetrahydride; potassium carbonate; In diethyl ether; ethanol; water; acetone;
DOI:10.1021/jo00284a018

Reference yield:

: 123291-85-0
2,2',2'',2'''-tetrakis(phenylmethoxy)-<1,1':3',1'':3'',1'''-quaterphenyl>-3,3'''-dicarboxylic acid

: 123291-87-2
2,2',2'',2'''-tetrakis(phenylmethoxy)-<1,1':3'',1'':1'''-quaterphenyl>-3,3'''-dimethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / K₂CO₃ / acetone / 15 h / Heating

2: 87 percent / LiAlH₄ / diethyl ether / 0.67 h / 0 °C

With lithium aluminium tetrahydride; potassium carbonate; In diethyl ether; acetone;
DOI:10.1021/jo00284a018