1-(2,6-dichloro-4-iodo-phenyl)-4-methyl-2,3,5,9,9b-pentaazacyclopenta[a]naphthalene

Base Information

Chemical Name:1-(2,6-dichloro-4-iodo-phenyl)-4-methyl-2,3,5,9,9b-pentaazacyclopenta[a]naphthalene
CAS No.:1426833-14-8
Molecular Formula:C₁₅H₈Cl₂IN₅
Molecular Weight:456.073
Hs Code.:

Synonyms:1-(2,6-dichloro-4-iodo-phenyl)-4-methyl-2,3,5,9,9b-pentaazacyclopenta[a]naphthalene

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Chemical Property of 1-(2,6-dichloro-4-iodo-phenyl)-4-methyl-2,3,5,9,9b-pentaazacyclopenta[a]naphthalene

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Technology Process of 1-(2,6-dichloro-4-iodo-phenyl)-4-methyl-2,3,5,9,9b-pentaazacyclopenta[a]naphthalene

There total 11 articles about 1-(2,6-dichloro-4-iodo-phenyl)-4-methyl-2,3,5,9,9b-pentaazacyclopenta[a]naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1426833-40-0
2,6-dichloro-4-iodo-benzoic acid N'-(2-methyl-pyrido[2,3-b]pyrazin-3-yl)-hydrazide

: 1426833-14-8
1-(2,6-dichloro-4-iodo-phenyl)-4-methyl-2,3,5,9,9b-pentaazacyclopenta[a]naphthalene

Guidance literature:: With trichlorophosphate; In 1,4-dioxane; at 90 ℃; for 1.5h;

Reference yield:

: 1098619-73-8
2,6-dichloro-4-iodo-benzoic acid methyl ester

: 1426833-14-8
1-(2,6-dichloro-4-iodo-phenyl)-4-methyl-2,3,5,9,9b-pentaazacyclopenta[a]naphthalene

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine; lithium iodide / water / 30 h / 130 °C

2: thionyl chloride / 3 h / 60 °C

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / 20 °C

4: trichlorophosphate / 1,4-dioxane / 1.5 h / 90 °C

With pyridine; thionyl chloride; N-ethyl-N,N-diisopropylamine; lithium iodide; trichlorophosphate; In 1,4-dioxane; water; N,N-dimethyl-formamide;

Reference yield:

: 1258298-01-9
2,6-dichloro-4-iodo-benzoic acid

: 1426833-14-8
1-(2,6-dichloro-4-iodo-phenyl)-4-methyl-2,3,5,9,9b-pentaazacyclopenta[a]naphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 3 h / 60 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / 20 °C

3: trichlorophosphate / 1,4-dioxane / 1.5 h / 90 °C

With thionyl chloride; N-ethyl-N,N-diisopropylamine; trichlorophosphate; In 1,4-dioxane; N,N-dimethyl-formamide;