Technology Process of C24H35N3O5
There total 5 articles about C24H35N3O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
1-[(tert-butoxycarbonyl)amino]cyclobutanecarboxylic acid;
With
dicyclohexyl-carbodiimide;
In
toluene;
at 0 - 10 ℃;
for 0.25h;
butyl (E)-3-(4-amino-3-(methylamino)phenyl)acrylate;
In
toluene;
at 0 - 25 ℃;
for 5h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: palladium diacetate; lithium chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl acetamide / 12 h / 110 °C / Inert atmosphere
2.1: hydrogen / water; toluene; methanol / 2 h / 20 - 25 °C / 3000.3 Torr
3.1: dicyclohexyl-carbodiimide / toluene / 0.25 h / 0 - 10 °C
3.2: 5 h / 0 - 25 °C
With
hydrogen; palladium diacetate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; lithium chloride;
In
methanol; N,N-dimethyl acetamide; water; toluene;
1.1: |Heck Reaction;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: palladium diacetate; lithium chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl acetamide / 12 h / 110 °C / Inert atmosphere
2.1: hydrogen / water; toluene; methanol / 2 h / 20 - 25 °C / 3000.3 Torr
3.1: dicyclohexyl-carbodiimide / toluene / 0.25 h / 0 - 10 °C
3.2: 5 h / 0 - 25 °C
With
hydrogen; palladium diacetate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; lithium chloride;
In
methanol; N,N-dimethyl acetamide; water; toluene;
1.1: |Heck Reaction;
