1,2-O-isopropyliden-3-O-(2-methoxyethyl)-6-O-(4-phenylbenzoyl)-α-D-allofuranose

Base Information

Chemical Name:1,2-O-isopropyliden-3-O-(2-methoxyethyl)-6-O-(4-phenylbenzoyl)-α-D-allofuranose
CAS No.:553664-31-6
Molecular Formula:C₂₅H₃₀O₈
Molecular Weight:458.508
Hs Code.:

Synonyms:1,2-O-isopropyliden-3-O-(2-methoxyethyl)-6-O-(4-phenylbenzoyl)-α-D-allofuranose

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Chemical Property of 1,2-O-isopropyliden-3-O-(2-methoxyethyl)-6-O-(4-phenylbenzoyl)-α-D-allofuranose

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Technology Process of 1,2-O-isopropyliden-3-O-(2-methoxyethyl)-6-O-(4-phenylbenzoyl)-α-D-allofuranose

There total 4 articles about 1,2-O-isopropyliden-3-O-(2-methoxyethyl)-6-O-(4-phenylbenzoyl)-α-D-allofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 14002-51-8
4-biphenyl-carboxylic acid chloride

: 553664-30-5
1,2-O-isopropyliden-3-O-(2-methoxyethyl)-α-D-allofuranose

: 553664-31-6
1,2-O-isopropyliden-3-O-(2-methoxyethyl)-6-O-(4-phenylbenzoyl)-α-D-allofuranose

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1002/hlca.200390013

Reference yield:

: 2595-05-3
Diacetone D-glucose

: 553664-31-6
1,2-O-isopropyliden-3-O-(2-methoxyethyl)-6-O-(4-phenylbenzoyl)-α-D-allofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / potassium hydroxide / dimethylsulfoxide / 7.5 h / 55 °C

2: 87 percent / AcOH / H₂O / 2 h / 40 °C

3: 70 percent / c-C₅H₅N / CH₂Cl₂ / 5 h / 20 °C

With pyridine; potassium hydroxide; acetic acid; In dichloromethane; water; dimethyl sulfoxide;
DOI:10.1002/hlca.200390013

Reference yield:

: 582-52-5
1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

: 553664-31-6
1,2-O-isopropyliden-3-O-(2-methoxyethyl)-6-O-(4-phenylbenzoyl)-α-D-allofuranose

Guidance literature:: Multi-step reaction with 4 steps

1.1: trifluoroacetic anhydride; triethylamine; DMSO / CH₂Cl₂ / -65 - 20 °C

1.2: 82 percent / sodium borohydride / methanol / 1 h / 0 °C

2.1: 95 percent / potassium hydroxide / dimethylsulfoxide / 7.5 h / 55 °C

3.1: 87 percent / AcOH / H₂O / 2 h / 40 °C

4.1: 70 percent / c-C₅H₅N / CH₂Cl₂ / 5 h / 20 °C

With pyridine; potassium hydroxide; acetic acid; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride; In dichloromethane; water; dimethyl sulfoxide;
DOI:10.1002/hlca.200390013