(S)-3-[(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyryl]-2-(4-methoxy-phenyl)-oxazolidine-4-carboxylic acid

Base Information

• Chemical Name: (S)-3-[(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyryl]-2-(4-methoxy-phenyl)-oxazolidine-4-carboxylic acid
• CAS No.: 204502-22-7
• Molecular Formula: C₃₁H₃₂N₂O₇
• Molecular Weight: 544.604

Synonyms:(S)-3-[(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyryl]-2-(4-methoxy-phenyl)-oxazolidine-4-carboxylic acid

Chemical Property of (S)-3-[(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyryl]-2-(4-methoxy-phenyl)-oxazolidine-4-carboxylic acid

Chemical Property:

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Technology Process of (S)-3-[(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyryl]-2-(4-methoxy-phenyl)-oxazolidine-4-carboxylic acid

There total 3 articles about (S)-3-[(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyryl]-2-(4-methoxy-phenyl)-oxazolidine-4-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-3-[(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyryl]-2-(4-methoxy-phenyl)-oxazolidine-4-carboxylic acid benzyl ester → (S)-3-[(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyryl]-2-(4-methoxy-phenyl)-oxazolidine-4-carboxylic acid (204502-22-7)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1021/ja962780a

Reference yield:

p-Anisaldehyde dimethyl acetal (2186-92-7) → (S)-3-[(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyryl]-2-(4-methoxy-phenyl)-oxazolidine-4-carboxylic acid (204502-22-7)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 2 h / Heating

2: H₂ / Pd/C / methanol

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol;

DOI:10.1021/ja962780a

Reference yield:

Fmoc-Val-Ser-OBn (186023-39-2) → (S)-3-[(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-methyl-butyryl]-2-(4-methoxy-phenyl)-oxazolidine-4-carboxylic acid (204502-22-7)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 2 h / Heating

2: H₂ / Pd/C / methanol

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol;

DOI:10.1021/ja962780a

upstream raw materials:

p-Anisaldehyde dimethyl acetal

Fmoc-Val-Ser-OBn

Downstream raw materials:

((S)-1-{(S)-2-(4-Methoxy-phenyl)-4-[(S)-1-(4-nitro-phenylcarbamoyl)-2-phenyl-ethylcarbamoyl]-oxazolidine-3-carbonyl}-2-methyl-propyl)-carbamic acid 9H-fluoren-9-ylmethyl ester

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