3-[(2-bromo-3-isopropyl-4,5-dimethoxyphenyl)(hydroxy)methyl]-2,4-dimethylphenol

Base Information

Chemical Name:3-[(2-bromo-3-isopropyl-4,5-dimethoxyphenyl)(hydroxy)methyl]-2,4-dimethylphenol
CAS No.:1357476-80-2
Molecular Formula:C₂₀H₂₅BrO₄
Molecular Weight:409.32
Hs Code.:

Synonyms:3-[(2-bromo-3-isopropyl-4,5-dimethoxyphenyl)(hydroxy)methyl]-2,4-dimethylphenol

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Chemical Property of 3-[(2-bromo-3-isopropyl-4,5-dimethoxyphenyl)(hydroxy)methyl]-2,4-dimethylphenol

Chemical Property:

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Technology Process of 3-[(2-bromo-3-isopropyl-4,5-dimethoxyphenyl)(hydroxy)methyl]-2,4-dimethylphenol

There total 10 articles about 3-[(2-bromo-3-isopropyl-4,5-dimethoxyphenyl)(hydroxy)methyl]-2,4-dimethylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1357476-78-8
(2-bromo-3-isopropyl-4,5-dimethoxyphenyl)(3-hydroxy-2,6-dimethylphenyl)methyl acetate

: 1357476-80-2
3-[(2-bromo-3-isopropyl-4,5-dimethoxyphenyl)(hydroxy)methyl]-2,4-dimethylphenol

Guidance literature:: With sodium hydroxide; In methanol; for 1h; Reflux;
DOI:10.1080/00397911.2010.518274

Reference yield:

: 1357476-75-5
3-[hydroxy(3-isopropyl-4,5-dimethoxyphenyl)methyl]-2,4-dimethylphenol

: 1357476-80-2
3-[(2-bromo-3-isopropyl-4,5-dimethoxyphenyl)(hydroxy)methyl]-2,4-dimethylphenol

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 14 h / 0 - 20 °C

2: N-Bromosuccinimide / acetonitrile / 96 h / 20 °C

3: water; potassium carbonate / methanol / 2 h / 20 °C

4: sodium hydroxide / methanol / 1 h / Reflux

With N-Bromosuccinimide; water; potassium carbonate; triethylamine; sodium hydroxide; In methanol; dichloromethane; acetonitrile;
DOI:10.1080/00397911.2010.518274

Reference yield:

: 1357476-73-3
3-[hydroxy(3-isopropenyl-4,5-dimethoxyphenyl)methyl]-2,4-dimethylphenol

: 1357476-80-2
3-[(2-bromo-3-isopropyl-4,5-dimethoxyphenyl)(hydroxy)methyl]-2,4-dimethylphenol

Guidance literature:: Multi-step reaction with 5 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 20 °C / 760.05 Torr

2: triethylamine / dichloromethane / 14 h / 0 - 20 °C

3: N-Bromosuccinimide / acetonitrile / 96 h / 20 °C

4: water; potassium carbonate / methanol / 2 h / 20 °C

5: sodium hydroxide / methanol / 1 h / Reflux

With N-Bromosuccinimide; palladium 10% on activated carbon; water; hydrogen; potassium carbonate; triethylamine; sodium hydroxide; In methanol; dichloromethane; acetonitrile;
DOI:10.1080/00397911.2010.518274