C₂₉H₃₉F₃N₆O₃

Base Information

Chemical Name:C₂₉H₃₉F₃N₆O₃
CAS No.:618900-61-1
Molecular Formula:C₂₉H₃₉F₃N₆O₃
Molecular Weight:576.662
Hs Code.:

C<sub>29</sub>H<sub>39</sub>F<sub>3</sub>N<sub>6</sub>O<sub>3</sub>

Synonyms:C₂₉H₃₉F₃N₆O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₃₉F₃N₆O₃

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Technology Process of C₂₉H₃₉F₃N₆O₃

There total 10 articles about C₂₉H₃₉F₃N₆O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 618900-60-0
C₂₉H₃₇F₃N₆O₅

: 618900-61-1
C₂₉H₃₉F₃N₆O₃

Guidance literature:: With hydrogen; Raney 2800 Nickel; In methanol; for 6h; under 1551.49 Torr;

Reference yield:

: 304873-62-9
(4-hydroxymethylpyridin-2-yl)carbamic acid tert-butyl ester

: 618900-61-1
C₂₉H₃₉F₃N₆O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; sodium bromide / dichloromethane; water / 1 h / 0 °C

2.1: acetic acid / dichloromethane / 0.67 h / 23 °C

2.2: 15 h / 23 °C

3.1: lithium hydroxide; water / tetrahydrofuran; methanol / 15 h / 23 °C

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 18 h / 70 °C

5.1: hydrogen / Raney_.(R). 2800 Nickel / methanol / 6 h / 1551.49 Torr

With lithium hydroxide; sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; water; hydrogen; sodium hydrogencarbonate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium bromide; Raney 2800 Nickel; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 695-34-1
2-Amino-4-methylpyridine

: 618900-61-1
C₂₉H₃₉F₃N₆O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: tert-butyl alcohol / 15 h / 23 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / 23 °C

2.2: 48 h / -78 - 23 °C

3.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; sodium bromide / dichloromethane; water / 1 h / 0 °C

4.1: acetic acid / dichloromethane / 0.67 h / 23 °C

4.2: 15 h / 23 °C

5.1: lithium hydroxide; water / tetrahydrofuran; methanol / 15 h / 23 °C

6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 18 h / 70 °C

7.1: hydrogen / Raney_.(R). 2800 Nickel / methanol / 6 h / 1551.49 Torr

With lithium hydroxide; sodium hypochlorite; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; water; hydrogen; sodium hydrogencarbonate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium bromide; Raney 2800 Nickel; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;