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Technology Process of tris(triphenylphosphine)monohydridopalladium perchlorate

tris(triphenylphosphine)monohydridopalladium perchlorate

Base Information
  • Chemical Name:tris(triphenylphosphine)monohydridopalladium perchlorate
  • CAS No.:117111-15-6
  • Molecular Formula:C54H46P3Pd*ClO4
  • Molecular Weight:993.751
  • Hs Code.:
tris(triphenylphosphine)monohydridopalladium perchlorate

Synonyms:tris(triphenylphosphine)monohydridopalladium perchlorate

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Chemical Property of tris(triphenylphosphine)monohydridopalladium perchlorate
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Technology Process of tris(triphenylphosphine)monohydridopalladium perchlorate

There total 1 articles about tris(triphenylphosphine)monohydridopalladium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

palladium diacetate
3375-31-3

palladium diacetate

HPd<sub>2</sub><sup>(1+)</sup>*4P(C<sub>6</sub>H<sub>5</sub>)3*CO*ClO<sub>4</sub><sup>(1-)</sup>={HPd<sub>2</sub>(P(C<sub>6</sub>H<sub>5</sub>)3)4(CO)(ClO<sub>4</sub>)}

HPd2(1+)*4P(C6H5)3*CO*ClO4(1-)={HPd2(P(C6H5)3)4(CO)(ClO4)}

tris(triphenylphosphine)monohydridopalladium perchlorate
117111-15-6

tris(triphenylphosphine)monohydridopalladium perchlorate

Guidance literature:
With perchloric acid; carbon monoxide; triphenylphosphine; In propan-1-ol; byproducts: CO2; charging reactor with 1 mmol Pd(CH3CO2)2, 3 mmol P(C6H5)3 and C3H7OH, stirring mixt. for 30 min under N2-atmosphere, then addn. of 4.3 N HClO4, bubbling CO through reactor (2 h); pptn., filtering, drying succesively with small portions of n-C4H9OH, C2H5OH and (C2H5)2O, drying under vac.; elem. anal.;
DOI:10.1007/BF00958348
upstream raw materials:

palladium diacetate

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