4-<(4S,5R,6R)-5-hydroxy-6-(benzoyloxymethyl)-1,3-dioxan-4-yl>-2,6-piperidinedione

Base Information

Chemical Name:4-<(4S,5R,6R)-5-hydroxy-6-(benzoyloxymethyl)-1,3-dioxan-4-yl>-2,6-piperidinedione
CAS No.:126267-12-7
Molecular Formula:C₁₇H₁₉NO₇
Molecular Weight:349.34
Hs Code.:

Synonyms:4-<(4S,5R,6R)-5-hydroxy-6-(benzoyloxymethyl)-1,3-dioxan-4-yl>-2,6-piperidinedione

Suppliers and Price of 4-<(4S,5R,6R)-5-hydroxy-6-(benzoyloxymethyl)-1,3-dioxan-4-yl>-2,6-piperidinedione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-<(4S,5R,6R)-5-hydroxy-6-(benzoyloxymethyl)-1,3-dioxan-4-yl>-2,6-piperidinedione

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-<(4S,5R,6R)-5-hydroxy-6-(benzoyloxymethyl)-1,3-dioxan-4-yl>-2,6-piperidinedione

There total 7 articles about 4-<(4S,5R,6R)-5-hydroxy-6-(benzoyloxymethyl)-1,3-dioxan-4-yl>-2,6-piperidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 98-88-4
benzoyl chloride

: 102487-45-6,102518-68-3,112419-11-1
(-)-4-<(4S,5R,6R)-5-hydroxy-6-(hydroxymethyl)-1,3-dioxan-4-yl>-2,6-piperidinedione

: 126267-12-7
4-<(4S,5R,6R)-5-hydroxy-6-(benzoyloxymethyl)-1,3-dioxan-4-yl>-2,6-piperidinedione

Guidance literature:: With pyridine; at -10 ℃; for 60h;

Reference yield: 92.0%

: 102487-45-6,102518-68-3,112419-11-1
4-((4S,5R,6R)-5-Hydroxy-6-hydroxymethyl-[1,3]dioxan-4-yl)-piperidine-2,6-dione

: 126267-12-7
4-<(4S,5R,6R)-5-hydroxy-6-(benzoyloxymethyl)-1,3-dioxan-4-yl>-2,6-piperidinedione

Guidance literature:: benzoylation;

Reference yield:

: 41341-99-5
3,5-di-O-benzyl-1,2-O-isopropylidene-α-D-xylofuranose

: 126267-12-7
4-<(4S,5R,6R)-5-hydroxy-6-(benzoyloxymethyl)-1,3-dioxan-4-yl>-2,6-piperidinedione

Guidance literature:: Multi-step reaction with 5 steps

1: 30percent HCl / tetrahydrofuran / 2 h / 20 °C

2: benzoic acid / toluene / 29 h / 22 °C

3: toluene, reflux, 30 min

4: H₂ / Pd/C / methanol

5: 94 percent / pyridine / 60 h / -10 °C

With pyridine; hydrogenchloride; hydrogen; benzoic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; toluene;