3-{2-[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-propionic acid; hydriodide

Base Information

Chemical Name:3-{2-[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-propionic acid; hydriodide
CAS No.:90957-05-4
Molecular Formula:C₂₃H₂₈N₄O₆S₂*HI
Molecular Weight:648.543
Hs Code.:

Synonyms:3-{2-[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-propionic acid; hydriodide

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Chemical Property of 3-{2-[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-propionic acid; hydriodide

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Technology Process of 3-{2-[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-propionic acid; hydriodide

There total 3 articles about 3-{2-[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-propionic acid; hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 90957-02-1
3-{2-[3-(4-Thiocarbamoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-propionic acid

: 74-88-4
methyl iodide

: 90957-05-4
3-{2-[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-propionic acid; hydriodide

Guidance literature:: In acetone; for 18h; Ambient temperature;

Reference yield:

: 90956-99-3
N-(Nα-Tosyl-4-cyanphenylalanyl)glycyl-β-alanin

: 90957-05-4
3-{2-[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-propionic acid; hydriodide

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / H₂S (gas) / pyridine; triethylamine / Ambient temperature

2: 81 percent / acetone / 18 h / Ambient temperature

With hydrogen sulfide; In pyridine; triethylamine; acetone;

Reference yield:

: 90282-17-0
N-(N_α-Tosyl-4-cyanphenylalanyl)glycin-(4-nitrophenylester)

: 90957-05-4
3-{2-[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetylamino}-propionic acid; hydriodide

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / 1M NaOH / pyridine; H₂O / 2 h / Ambient temperature

2: 70 percent / H₂S (gas) / pyridine; triethylamine / Ambient temperature

3: 81 percent / acetone / 18 h / Ambient temperature

With sodium hydroxide; hydrogen sulfide; In pyridine; water; triethylamine; acetone;