benzyl 2-(benzyloxycarbonylamino)-2-deoxy-β-D-xylofuranoside

Base Information

• Chemical Name: benzyl 2-(benzyloxycarbonylamino)-2-deoxy-β-D-xylofuranoside
• CAS No.: 66166-90-3
• Molecular Formula: C₂₀H₂₃NO₆
• Molecular Weight: 373.406
• Mol file: 66166-90-3.mol

Synonyms:benzyl 2-(benzyloxycarbonylamino)-2-deoxy-β-D-xylofuranoside

Chemical Property of benzyl 2-(benzyloxycarbonylamino)-2-deoxy-β-D-xylofuranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzyl 2-(benzyloxycarbonylamino)-2-deoxy-β-D-xylofuranoside

There total 3 articles about benzyl 2-(benzyloxycarbonylamino)-2-deoxy-β-D-xylofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

benzyl 2-(benzyloxycarbonyl)amino-2-deoxy-β-D-glucofuranoside (42890-17-5) → benzyl 2-(benzyloxycarbonylamino)-2-deoxy-β-D-xylofuranoside (66166-90-3)

Guidance literature:

With sodium periodate; In methanol; at 0 ℃; for 2h;

DOI:10.1016/S0008-6215(00)84865-X

Reference yield:

benzyl 2-(benzyloxycarbonyl)amino-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside (58886-40-1) → benzyl 2-(benzyloxycarbonylamino)-2-deoxy-β-D-xylofuranoside (66166-90-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / aq. acetic acid / 3 h / 40 °C

2: 83 percent / 0.2M aqueous sodium metaperiodate / methanol / 2 h / 0 °C

With sodium periodate; In methanol; acetic acid;

DOI:10.1016/S0008-6215(00)84865-X

Reference yield:

→ benzyl 2-(benzyloxycarbonylamino)-2-deoxy-β-D-xylofuranoside (66166-90-3)

Guidance literature:

Benzyl-2-(benzyloxycarbonyl)-amino-2-deoxy-β-D-glucofuranosid (II), 1.) NaIO4 -> /BRN= 403237/, 2.) Red. mit NaBH4;

upstream raw materials:

benzyl 2-(benzyloxycarbonyl)amino-2-deoxy-β-D-glucofuranoside

benzyl 2-(benzyloxycarbonyl)amino-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

Downstream raw materials:

benzyl 2-acetamido-5-azido-2,5-dideoxy-β-D-xylofuranoside

benzyl 2-acetamido-2-deoxy-5-O-tosyl-β-D-xylofuranoside

benzyl 2-acetamido-5-amino-2,5-dideoxy-β-D-xylofuranoside monoacetate

benzyl 2-acetamido-5-amino-2,5-dideoxy-β-D-ribofuranoside monoacetate