benzyl 2-(benzyloxycarbonylamino)-2-deoxy-3,5-di-O-mesyl-β-D-xylofuranoside

Base Information

Chemical Name:benzyl 2-(benzyloxycarbonylamino)-2-deoxy-3,5-di-O-mesyl-β-D-xylofuranoside
CAS No.:74593-10-5
Molecular Formula:C₂₂H₂₇NO₁₀S₂
Molecular Weight:529.589
Hs Code.:

Synonyms:benzyl 2-(benzyloxycarbonylamino)-2-deoxy-3,5-di-O-mesyl-β-D-xylofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 2-(benzyloxycarbonylamino)-2-deoxy-3,5-di-O-mesyl-β-D-xylofuranoside

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Technology Process of benzyl 2-(benzyloxycarbonylamino)-2-deoxy-3,5-di-O-mesyl-β-D-xylofuranoside

There total 1 articles about benzyl 2-(benzyloxycarbonylamino)-2-deoxy-3,5-di-O-mesyl-β-D-xylofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 66166-90-3
benzyl 2-(benzyloxycarbonylamino)-2-deoxy-β-D-xylofuranoside

: 124-63-0
methanesulfonyl chloride

: 74593-10-5
benzyl 2-(benzyloxycarbonylamino)-2-deoxy-3,5-di-O-mesyl-β-D-xylofuranoside

Guidance literature:: With pyridine; at 0 ℃; for 3h;
DOI:10.1016/S0008-6215(00)85674-8

Reference yield: 93.0%

: 74593-10-5
benzyl 2-(benzyloxycarbonylamino)-2-deoxy-3,5-di-O-mesyl-β-D-xylofuranoside

: 74593-11-6
benzyl 3,5-diazido-2-(benzyloxycarbonylamino)-2,3,5-trideoxy-β-D-ribofuranoside

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 80 - 85 ℃; for 12h;
DOI:10.1016/S0008-6215(00)85674-8

Reference yield:

: 74593-10-5
benzyl 2-(benzyloxycarbonylamino)-2-deoxy-3,5-di-O-mesyl-β-D-xylofuranoside

: 74593-08-1
benzyl 2-acetamido-3,5-diazido-2,3,5-trideoxy-β-D-xylofuranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) hydrogen / 1.) 10percent Pd-C / 1.) 1,4-dioxane/methanol, room temperature, 2.5 h; 2.)methanol, room temperature, 30 min

2: 1.) sodium azide / 1.) N,N-dimethylformamide, 90 degC; 2.) N,N-dimethylformamide, 90 degC

3: 68 percent / hydrochlorid acid, Amberlite IRA-45 resin / acetic acid / 4 h / 50 °C

4: 80 percent / pyridine / 3 h / 0 °C

5: 56 percent / sodium azide / dimethylformamide / 48 h / 120 °C

With pyridine; hydrogenchloride; sodium azide; Amberlite IRA-45 resin; hydrogen; palladium on activated charcoal; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)85674-8