tokaramide A

Base Information

• Chemical Name: tokaramide A
• CAS No.: 928821-35-6
• Molecular Formula: C₂₃H₃₆N₆O₅
• Molecular Weight: 476.576
• Mol file: 928821-35-6.mol

Synonyms:tokaramide A

Chemical Property of tokaramide A

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tokaramide A

There total 23 articles about tokaramide A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

C25H41N7O6 (1345676-76-7) → tokaramide A (928821-35-6)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃;

DOI:10.1016/j.tet.2011.09.116

Reference yield: 4.0%

C37H56N6O10S (1345676-74-5) → C23H34N6O4 (1345676-75-6) + tokaramide A (928821-35-6)

Guidance literature:

With trifluoroacetic acid; for 2h;

DOI:10.1016/j.tet.2011.09.116

Reference yield:

C38H58N7O11PolS → tokaramide A (928821-35-6)

Guidance literature:

C₃₈H₅₈N₇O₁₁PolS; With trifluoroacetic acid; for 2h; solid phase reaction;

With lithium aluminium tetrahydride; In tetrahydrofuran; for 0.5h; solid phase reaction;

DOI:10.1016/j.tet.2011.09.116

upstream raw materials:

N-α-(9-fluorenylmethyloxycarbonyl)-N'-ω'-(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-L-arginine-N,O-dimethylhydroxyamide

H-Arg(Mtr)-N(OMe)Me

C₃₈H₅₀N₆O₈S

Fmoc-Val-Val-Arg(Mtr)-N(OMe)Me

Refernces