7,8-dimethoxy-2-{4-((4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)methyl)-1H-1,2,3-triazol-1-yl}-(11aS)-1,2,3,11a-tetrahydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-5-one

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Chemical Name:7,8-dimethoxy-2-{4-((4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)methyl)-1H-1,2,3-triazol-1-yl}-(11aS)-1,2,3,11a-tetrahydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-5-one
CAS No.:1335131-06-0
Molecular Formula:C₃₃H₃₁N₅O₇
Molecular Weight:609.638
Hs Code.:

7,8-dimethoxy-2-{4-((4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)methyl)-1H-1,2,3-triazol-1-yl}-(11aS)-1,2,3,11a-tetrahydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-5-one

Synonyms:7,8-dimethoxy-2-{4-((4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)methyl)-1H-1,2,3-triazol-1-yl}-(11aS)-1,2,3,11a-tetrahydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-5-one

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Chemical Property of 7,8-dimethoxy-2-{4-((4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)methyl)-1H-1,2,3-triazol-1-yl}-(11aS)-1,2,3,11a-tetrahydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-5-one

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Technology Process of 7,8-dimethoxy-2-{4-((4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)methyl)-1H-1,2,3-triazol-1-yl}-(11aS)-1,2,3,11a-tetrahydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-5-one

There total 5 articles about 7,8-dimethoxy-2-{4-((4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)methyl)-1H-1,2,3-triazol-1-yl}-(11aS)-1,2,3,11a-tetrahydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₇H₄₃N₅O₇S₂

: 1335131-06-0
7,8-dimethoxy-2-{4-((4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)methyl)-1H-1,2,3-triazol-1-yl}-(11aS)-1,2,3,11a-tetrahydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-5-one

Guidance literature:: With calcium carbonate; mercury dichloride; In water; acetonitrile; at 20 ℃; for 12h;
DOI:10.1016/j.ejmech.2011.05.050

Reference yield:

: 1335130-94-3
(E)-1-(2-hydroxyphenyl)-3-(3-methoxy-4-(prop-2-ynyloxy)phenyl)prop-2-en-1-one

: 1335131-06-0
7,8-dimethoxy-2-{4-((4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)methyl)-1H-1,2,3-triazol-1-yl}-(11aS)-1,2,3,11a-tetrahydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-5-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 12 h

2.1: tin(II) chloride dihdyrate / methanol / 2 h / Reflux

2.2: pH 8

3.1: calcium carbonate; mercury dichloride / water; acetonitrile / 12 h / 20 °C

With copper(ll) sulfate pentahydrate; tin(II) chloride dihdyrate; sodium L-ascorbate; calcium carbonate; mercury dichloride; In methanol; water; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.ejmech.2011.05.050

Reference yield:

: 1335130-95-4
C₃₇H₄₁N₅O₉S₂

: 1335131-06-0
7,8-dimethoxy-2-{4-((4-((E)-3-(2-hydroxyphenyl)-3-oxoprop-1-enyl)-2-methoxyphenoxy)methyl)-1H-1,2,3-triazol-1-yl}-(11aS)-1,2,3,11a-tetrahydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-5-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: tin(II) chloride dihdyrate / methanol / 2 h / Reflux

1.2: pH 8

2.1: calcium carbonate; mercury dichloride / water; acetonitrile / 12 h / 20 °C

With tin(II) chloride dihdyrate; calcium carbonate; mercury dichloride; In methanol; water; acetonitrile;
DOI:10.1016/j.ejmech.2011.05.050