4,4'-dithiobis-(2-trifluoromethylphenoxyacetic acid)

Base Information

Chemical Name:4,4'-dithiobis-(2-trifluoromethylphenoxyacetic acid)
CAS No.:1354482-55-5
Molecular Formula:C₁₈H₁₂F₆O₆S₂
Molecular Weight:502.412
Hs Code.:

Synonyms:4,4'-dithiobis-(2-trifluoromethylphenoxyacetic acid)

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Chemical Property of 4,4'-dithiobis-(2-trifluoromethylphenoxyacetic acid)

Chemical Property:

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Technology Process of 4,4'-dithiobis-(2-trifluoromethylphenoxyacetic acid)

There total 4 articles about 4,4'-dithiobis-(2-trifluoromethylphenoxyacetic acid) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₁H₁₀F₃N₂O₃⁽¹⁺⁾*Cl^(1-)

: 1354482-55-5
4,4'-dithiobis-(2-trifluoromethylphenoxyacetic acid)

Guidance literature:: With sodium sulfide; sodium hydroxide; sulfur; In water; at 5 ℃; Heating / reflux;

Reference yield:

: 719293-86-4
(4-nitro-2-trifluoromethyl-phenoxy)-acetic acid ethyl ester

: 1354482-55-5
4,4'-dithiobis-(2-trifluoromethylphenoxyacetic acid)

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / 5%-palladium/activated carbon / ethanol / 3 h

2: hydrogenchloride; sodium nitrite / water / 0.08 h / 5 °C

3: sodium sulfide; sodium hydroxide; sulfur / water / 5 °C / Heating / reflux

With hydrogenchloride; sodium sulfide; sodium hydroxide; hydrogen; sulfur; sodium nitrite; 5%-palladium/activated carbon; In ethanol; water;

Reference yield:

: 1548-61-4
4-nitro-2-(trifluoromethyl)phenol

: 1354482-55-5
4,4'-dithiobis-(2-trifluoromethylphenoxyacetic acid)

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / butanone / 10 h / Heating / reflux

2: hydrogen / 5%-palladium/activated carbon / ethanol / 3 h

3: hydrogenchloride; sodium nitrite / water / 0.08 h / 5 °C

4: sodium sulfide; sodium hydroxide; sulfur / water / 5 °C / Heating / reflux

With hydrogenchloride; sodium sulfide; sodium hydroxide; hydrogen; potassium carbonate; sulfur; sodium nitrite; 5%-palladium/activated carbon; In ethanol; water; butanone;