4,4'-dithiobis-(2-trifluoromethylphenoxyacetic acid) diethyl ester

Base Information

Chemical Name:4,4'-dithiobis-(2-trifluoromethylphenoxyacetic acid) diethyl ester
CAS No.:719293-88-6
Molecular Formula:C₂₂H₂₀F₆O₆S₂
Molecular Weight:558.52
Hs Code.:

Synonyms:4,4'-dithiobis-(2-trifluoromethylphenoxyacetic acid) diethyl ester

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Chemical Property of 4,4'-dithiobis-(2-trifluoromethylphenoxyacetic acid) diethyl ester

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Technology Process of 4,4'-dithiobis-(2-trifluoromethylphenoxyacetic acid) diethyl ester

There total 5 articles about 4,4'-dithiobis-(2-trifluoromethylphenoxyacetic acid) diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1354482-55-5
4,4'-dithiobis-(2-trifluoromethylphenoxyacetic acid)

: 64-17-5
ethanol

: 719293-88-6
4,4'-dithiobis-(2-trifluoromethylphenoxyacetic acid) diethyl ester

Guidance literature:: With sulfuric acid; for 8h; Heating / reflux;

Reference yield:

: 719293-86-4
(4-nitro-2-trifluoromethyl-phenoxy)-acetic acid ethyl ester

: 719293-88-6
4,4'-dithiobis-(2-trifluoromethylphenoxyacetic acid) diethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen / 5%-palladium/activated carbon / ethanol / 3 h

2: hydrogenchloride; sodium nitrite / water / 0.08 h / 5 °C

3: sodium sulfide; sodium hydroxide; sulfur / water / 5 °C / Heating / reflux

4: sulfuric acid / 8 h / Heating / reflux

With hydrogenchloride; sodium sulfide; sodium hydroxide; sulfuric acid; hydrogen; sulfur; sodium nitrite; 5%-palladium/activated carbon; In ethanol; water;

Reference yield:

: 1548-61-4
4-nitro-2-(trifluoromethyl)phenol

: 719293-88-6
4,4'-dithiobis-(2-trifluoromethylphenoxyacetic acid) diethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / butanone / 10 h / Heating / reflux

2: hydrogen / 5%-palladium/activated carbon / ethanol / 3 h

3: hydrogenchloride; sodium nitrite / water / 0.08 h / 5 °C

4: sodium sulfide; sodium hydroxide; sulfur / water / 5 °C / Heating / reflux

5: sulfuric acid / 8 h / Heating / reflux

With hydrogenchloride; sodium sulfide; sodium hydroxide; sulfuric acid; hydrogen; potassium carbonate; sulfur; sodium nitrite; 5%-palladium/activated carbon; In ethanol; water; butanone;