C₄₈H₅₄N₄O₅

Base Information

Chemical Name:C₄₈H₅₄N₄O₅
CAS No.:1448802-23-0
Molecular Formula:C₄₈H₅₄N₄O₅
Molecular Weight:766.981
Hs Code.:

C<sub>48</sub>H<sub>54</sub>N<sub>4</sub>O<sub>5</sub>

Synonyms:C₄₈H₅₄N₄O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₈H₅₄N₄O₅

Chemical Property:

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Technology Process of C₄₈H₅₄N₄O₅

There total 12 articles about C₄₈H₅₄N₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1448802-20-7
C₂₄H₂₈N₂O₃

: 1448802-22-9
C₂₄H₂₇BrN₂O₂

: 1448802-23-0
C₄₈H₅₄N₄O₅

Guidance literature:: With palladium diacetate; caesium carbonate; 2'-(di-tert-butylphosphanyl)-N,N-dimethyl-[1,1'-biphenyl]-2-amine; Trimethylacetic acid; In toluene; 1,3,5-trimethyl-benzene; at 130 ℃; for 14h; Inert atmosphere;
DOI:10.1002/anie.201208297

Reference yield:

: 1448802-19-4
Cbz-lycodine

: 1448802-23-0
C₄₈H₅₄N₄O₅

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

2: palladium diacetate; 2'-(di-tert-butylphosphanyl)-N,N-dimethyl-[1,1'-biphenyl]-2-amine; caesium carbonate; Trimethylacetic acid / 1,3,5-trimethyl-benzene; toluene / 14 h / 130 °C / Inert atmosphere

With palladium diacetate; caesium carbonate; 3-chloro-benzenecarboperoxoic acid; 2'-(di-tert-butylphosphanyl)-N,N-dimethyl-[1,1'-biphenyl]-2-amine; Trimethylacetic acid; In dichloromethane; toluene; 1,3,5-trimethyl-benzene;
DOI:10.1002/anie.201208297

Reference yield:

: C₂₄H₂₆N₂O₃

: 1448802-23-0
C₄₈H₅₄N₄O₅

Guidance literature:: Multi-step reaction with 5 steps

1: Daicel Chiral-Pak AS / ethanol; hexane; diethylamine / Resolution of racemate

2: boron trifluoride diethyl etherate / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

3: triphenylstannane; 2,2'-azobis(isobutyronitrile) / toluene / 0.5 h / 110 °C / Inert atmosphere

4: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

5: palladium diacetate; 2'-(di-tert-butylphosphanyl)-N,N-dimethyl-[1,1'-biphenyl]-2-amine; caesium carbonate; Trimethylacetic acid / 1,3,5-trimethyl-benzene; toluene / 14 h / 130 °C / Inert atmosphere

With 2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; triphenylstannane; palladium diacetate; caesium carbonate; 3-chloro-benzenecarboperoxoic acid; 2'-(di-tert-butylphosphanyl)-N,N-dimethyl-[1,1'-biphenyl]-2-amine; Trimethylacetic acid; In ethanol; hexane; dichloromethane; diethylamine; toluene; 1,3,5-trimethyl-benzene;
DOI:10.1002/anie.201208297