5-valeraldehyde ethylene acetal

Base Information

Chemical Name:5-valeraldehyde ethylene acetal
CAS No.:93185-14-9
Molecular Formula:C₁₉H₂₉NO₂
Molecular Weight:303.445
Hs Code.:

5-<N-(1-phenylcycloheksyl)amino>valeraldehyde ethylene acetal

Synonyms:5-valeraldehyde ethylene acetal

Suppliers and Price of 5-valeraldehyde ethylene acetal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-valeraldehyde ethylene acetal

Chemical Property:

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Technology Process of 5-valeraldehyde ethylene acetal

There total 4 articles about 5-valeraldehyde ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 1934-71-0
IEM 1921

: 87227-41-6
2-(4-bromobutyl)-1,3-dioxolane

: 93185-14-9
5-valeraldehyde ethylene acetal

Guidance literature:: With calcium carbonate; In N,N-dimethyl-formamide; for 36h; Ambient temperature;
DOI:10.1021/jm00379a011

Reference yield:

: 1934-58-3
Benzyl-(1-phenyl-cyclohexyl)-amine; hydrochloride

: 93185-14-9
5-valeraldehyde ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: H₂, conc. aq.HCl / 10percent Pd-C / ethanol / 24 h / 50 °C / 2585.7 Torr

2: 39 percent / CaCO₃ / dimethylformamide / 36 h / Ambient temperature

With hydrogenchloride; hydrogen; calcium carbonate; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00379a011

Reference yield:

: 5414-21-1
5-bromopentan-1-nitrile

: 93185-14-9
5-valeraldehyde ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / 75percent HCOOH, Raney Ni / 6 h / 65 °C

2: 81 percent / p-CH₃-C₆H₄-SO₃H / benzene / 8 h / Heating

3: 39 percent / CaCO₃ / dimethylformamide / 36 h / Ambient temperature

With formic acid; nickel; toluene-4-sulfonic acid; calcium carbonate; In N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00379a011