K⁽¹⁺⁾*(C₁₂H₂₄O₆)*{Co(NC₅H₂C₆H₅)4(SC₆H₅)}^(1-)*HSC₆H₅=K(C₁₂H₂₄O₆){Co(NC₅H₂C₆H₅)4(SC₆H₅)}(HSC₆H₅)

Base Information

• Chemical Name: K⁽¹⁺⁾*(C₁₂H₂₄O₆)*{Co(NC₅H₂C₆H₅)4(SC₆H₅)}^(1-)*HSC₆H₅=K(C₁₂H₂₄O₆){Co(NC₅H₂C₆H₅)4(SC₆H₅)}(HSC₆H₅)
• CAS No.: 98652-73-4
• Molecular Formula: C₆H₆S*C₁₂H₂₄O₆*C₅₀H₃₃CoN₄S*K
• Molecular Weight: 1194.49

Synonyms:K⁽¹⁺⁾*(C₁₂H₂₄O₆)*{Co(NC₅H₂C₆H₅)4(SC₆H₅)}^(1-)*HSC₆H₅=K(C₁₂H₂₄O₆){Co(NC₅H₂C₆H₅)4(SC₆H₅)}(HSC₆H₅)

Chemical Property of K⁽¹⁺⁾*(C₁₂H₂₄O₆)*{Co(NC₅H₂C₆H₅)4(SC₆H₅)}^(1-)*HSC₆H₅=K(C₁₂H₂₄O₆){Co(NC₅H₂C₆H₅)4(SC₆H₅)}(HSC₆H₅)

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Technology Process of K⁽¹⁺⁾*(C₁₂H₂₄O₆)*{Co(NC₅H₂C₆H₅)4(SC₆H₅)}^(1-)*HSC₆H₅=K(C₁₂H₂₄O₆){Co(NC₅H₂C₆H₅)4(SC₆H₅)}(HSC₆H₅)

There total 1 articles about K⁽¹⁺⁾*(C₁₂H₂₄O₆)*{Co(NC₅H₂C₆H₅)4(SC₆H₅)}^(1-)*HSC₆H₅=K(C₁₂H₂₄O₆){Co(NC₅H₂C₆H₅)4(SC₆H₅)}(HSC₆H₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cobalt(II) 5,10,15,20-tetraphenylporphyrin (14172-90-8) + 18-crown-6 ether (17455-13-9) + thiophenol (108-98-5) → K(1+)*(C12H24O6)*{Co(NC5H2C6H5)4(SC6H5)}(1-)*HSC6H5=K(C12H24O6){Co(NC5H2C6H5)4(SC6H5)}(HSC6H5) (98652-73-4)

Guidance literature:

With potassium hydride; In benzene; 18-crown-6 ether, potassium hydride and benzenethiol dissolved in degassed benzene, soln. stirred overnight, benzene soln. of Co complex added; concd. under reduced pressure, filtered, washed with benzene, elem. anal.;

DOI:10.1021/ja00309a017

Reference yield:

K(1+)*(C12H24O6)*{Co(NC5H2C6H5)4(SC6H5)}(1-)*HSC6H5=K(C12H24O6){Co(NC5H2C6H5)4(SC6H5)}(HSC6H5) (98652-73-4) → Co(tetraphenylporphyrin)(benzenethiol)dioxygen (98677-71-5)

Guidance literature:

With oxygen; In dichloromethane; CH2Cl2 soln. of Co complex satd. with O2 at 185 K and warmed to 225 K;

DOI:10.1021/ja00309a017

upstream raw materials:

cobalt(II) 5,10,15,20-tetraphenylporphyrin

18-crown-6 ether

thiophenol

Downstream raw materials:

Co(tetraphenylporphyrin)(benzenethiol)dioxygen

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