1-Phenylmethyl-L-histidine methyl ester monohydrochloride

Base Information

• Chemical Name: 1-Phenylmethyl-L-histidine methyl ester monohydrochloride
• CAS No.: 274927-61-6
• Molecular Formula: C14H17 N3 O2 . Cl H
• Molecular Weight: 295.77
• Hs Code.: 2933290090
• Mol file: 274927-61-6.mol

Synonyms:L-Histidine,1-(phenylmethyl)-,methylester,monohydrochloride;1-PHENYLMETHYL-L-HISTIDINE METHYL ESTER MONOHYDROCHLORIDE

Chemical Property of 1-Phenylmethyl-L-histidine methyl ester monohydrochloride

Chemical Property:

• Vapor Pressure: 7.81E-08mmHg at 25°C
• Boiling Point: 436.9oC at 760 mmHg
• Flash Point: 218oC
• PSA: 70.14000
• LogP: 2.47650
• Storage Temp.: Hygroscopic, -20°C Freezer, Under inert atmosphere
• Solubility.: Aqueous Acid (Slightly) DMSO (Slightly), Methanol (Slightly)

Purity/Quality:

97% ^*data from raw suppliers

(S)-Methyl 2-amino-3-(1-benzyl-1H-imidazol-4-yl)propanoate hydrochloride 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Phenylmethyl-L-histidine methyl ester monohydrochloride

There total 1 articles about 1-Phenylmethyl-L-histidine methyl ester monohydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol hydrochloride (101752-05-0) + Boc-His(Bzl)-OH (20898-44-6,81018-79-3) → Nτ-benzyl-L-histidine methyl ester hydrochloride (274927-61-6)

Guidance literature:

at 80 ℃; for 5h;

Reference yield: 56.3%

C15H17NO7 (1155873-40-7) + Nτ-benzyl-L-histidine methyl ester hydrochloride (274927-61-6) → C29H34N4O9 (1331961-17-1)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃;

DOI:10.1002/ardp.201100109

upstream raw materials:

methanol hydrochloride

Boc-His(Bzl)-OH

Downstream raw materials:

C₂₉H₃₄N₄O₉

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