1-Azabicyclo[2.2.2]oct-2-ene-3-carboxylic acid methyl ester hydrochloride

Base Information

• Chemical Name: 1-Azabicyclo[2.2.2]oct-2-ene-3-carboxylic acid methyl ester hydrochloride
• CAS No.: 33630-87-4
• Molecular Formula: C₉H₁₃NO₂*ClH
• Molecular Weight: 203.669
• Hs Code.: 2933990090
• Mol file: 33630-87-4.mol

Synonyms:1-Azabicyclo[2.2.2]oct-2-ene-3-carboxylicacid, methyl ester, hydrochloride (6CI,8CI,9CI);Methyl2,3-dehydroquinuclidine-3-carboxylate hydrochloride;

Chemical Property of 1-Azabicyclo[2.2.2]oct-2-ene-3-carboxylic acid methyl ester hydrochloride

Chemical Property:

• Vapor Pressure: 0.00193mmHg at 25°C
• Melting Point: 178-179 °C (decomp)(Solv: acetone (67-64-1))
• Boiling Point: 287.1 °C at 760 mmHg
• Flash Point: 127.4 °C
• PSA: 29.54000
• LogP: 1.50880

Purity/Quality:

97% ^*data from raw suppliers

Methyl1-azabicyclo[2.2.2]oct-2-ene-3-carboxylatehydrochloride 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Azabicyclo[2.2.2]oct-2-ene-3-carboxylic acid methyl ester hydrochloride

There total 2 articles about 1-Azabicyclo[2.2.2]oct-2-ene-3-carboxylic acid methyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

→ 1-aza-bicyclo[2.2.2]oct-2-ene-3-carboxylic acid methyl ester; hydrochloride (33630-87-4)

Guidance literature:

Reference yield:

3-hydroxy-3-methoxycarbonyl-1-azabicyclo[2.2.2]octane (57598-88-6) → 1-aza-bicyclo[2.2.2]oct-2-ene-3-carboxylic acid methyl ester; hydrochloride (33630-87-4)

Guidance literature:

With thionyl chloride;

upstream raw materials:

3-hydroxy-3-methoxycarbonyl-1-azabicyclo[2.2.2]octane

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