trans-3-phenyl-2-propenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

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Chemical Name:trans-3-phenyl-2-propenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside
CAS No.:508194-07-8
Molecular Formula:C₂₃H₂₉NO₉
Molecular Weight:463.485
Hs Code.:

Synonyms:trans-3-phenyl-2-propenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-3-phenyl-2-propenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

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Technology Process of trans-3-phenyl-2-propenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

There total 1 articles about trans-3-phenyl-2-propenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 3068-34-6
Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester

: 508194-07-8
trans-3-phenyl-2-propenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; mercury(II) cyanide; In nitromethane; toluene; at 20 ℃;
DOI:10.1016/S0957-4166(02)00649-3

Reference yield:

: 508194-07-8
trans-3-phenyl-2-propenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

: 194035-36-4
N-[(2R,3R,4R,5S,6R)-4,5-Dihydroxy-6-hydroxymethyl-2-((E)-3-phenyl-allyloxy)-tetrahydro-pyran-3-yl]-acetamide

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 0.5h;
DOI:10.1016/S0957-4166(02)00649-3

Reference yield:

: 508194-07-8
trans-3-phenyl-2-propenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

: (2S,3S)-2,3-epoxy-3-phenylpropyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

: (2R,3R)-2,3-epoxy-3-phenylpropyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 10 ℃; for 144h; Title compound not separated from byproducts;
DOI:10.1016/S0957-4166(02)00649-3